4-(2-chloro-phenyl)-9-methyl-6H-thieno[3,2-f][1,2,4]triazolo[4,3-a][1,4]diazepine

Base Information

Chemical Name:4-(2-chloro-phenyl)-9-methyl-6H-thieno[3,2-f][1,2,4]triazolo[4,3-a][1,4]diazepine
CAS No.:54123-29-4
Molecular Formula:C₁₅H₁₁ClN₄S
Molecular Weight:314.798
Hs Code.:

4-(2-chloro-phenyl)-9-methyl-6<i>H</i>-thieno[3,2-<i>f</i>][1,2,4]triazolo[4,3-<i>a</i>][1,4]diazepine

Synonyms:4-(2-chloro-phenyl)-9-methyl-6H-thieno[3,2-f][1,2,4]triazolo[4,3-a][1,4]diazepine

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Chemical Property of 4-(2-chloro-phenyl)-9-methyl-6H-thieno[3,2-f][1,2,4]triazolo[4,3-a][1,4]diazepine

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Technology Process of 4-(2-chloro-phenyl)-9-methyl-6H-thieno[3,2-f][1,2,4]triazolo[4,3-a][1,4]diazepine

There total 5 articles about 4-(2-chloro-phenyl)-9-methyl-6H-thieno[3,2-f][1,2,4]triazolo[4,3-a][1,4]diazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54123-28-3
5-(2-chloro-phenyl)-1,3-dihydro-thieno[2,3-e][1,4]diazepin-2-one hydrazone

: 75-36-5
acetyl chloride

: 54123-29-4
4-(2-chloro-phenyl)-9-methyl-6H-thieno[3,2-f][1,2,4]triazolo[4,3-a][1,4]diazepine

Guidance literature:: With sodium hydrogencarbonate; In dichloromethane; water; butan-1-ol;

Reference yield:

: 67727-22-4
5-(2-chloro-phenyl)-1,3-dihydro-thieno[2,3-e][1,4]diazepine-2-thione

: 54123-29-4
4-(2-chloro-phenyl)-9-methyl-6H-thieno[3,2-f][1,2,4]triazolo[4,3-a][1,4]diazepine

Guidance literature:: Multi-step reaction with 2 steps

1: N₂H₄*H₂O / methanol / Ambient temperature

2: AcOH / benzene

With hydrazine hydrate; acetic acid; In methanol; benzene;

Reference yield:

: 36811-58-2
5-(2-chlorophenyl)-1,3-dihydro-2H-thieno[2,3-e][4,1]diazepin-2-one

: 54123-29-4
4-(2-chloro-phenyl)-9-methyl-6H-thieno[3,2-f][1,2,4]triazolo[4,3-a][1,4]diazepine

Guidance literature:: Multi-step reaction with 3 steps

1: P₂S₅, Py / 1 h

2: N₂H₄*H₂O / methanol / Ambient temperature

3: AcOH / benzene

With pyridine; tetraphosphorus decasulfide; hydrazine hydrate; acetic acid; In methanol; benzene;