tris(4-phenylphosphinato-3-methyl-3-azabutyl)amine trihydrochloride monohydrate

Base Information

Chemical Name:tris(4-phenylphosphinato-3-methyl-3-azabutyl)amine trihydrochloride monohydrate
CAS No.:777833-09-7
Molecular Formula:C₃₀H₄₅N₄O₆P₃
Molecular Weight:650.632
Hs Code.:

Synonyms:tris(4-phenylphosphinato-3-methyl-3-azabutyl)amine trihydrochloride monohydrate

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Chemical Property of tris(4-phenylphosphinato-3-methyl-3-azabutyl)amine trihydrochloride monohydrate

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Technology Process of tris(4-phenylphosphinato-3-methyl-3-azabutyl)amine trihydrochloride monohydrate

There total 1 articles about tris(4-phenylphosphinato-3-methyl-3-azabutyl)amine trihydrochloride monohydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1779-48-2
phenylphosphinic acid

: 65604-89-9
tris[2-(methylamino)ethyl]amine

: 777833-09-7
tris(4-phenylphosphinato-3-methyl-3-azabutyl)amine trihydrochloride monohydrate

Guidance literature:: With hydrogenchloride; for 5h; Heating;
DOI:10.1021/ja961633+

Reference yield: 78.0%

: ytterbium(III) nitrate hydrate

: 777833-09-7
tris(4-phenylphosphinato-3-methyl-3-azabutyl)amine trihydrochloride monohydrate

: [Yb(tris(4-phenylphosphinato-3-methyl-3-azabutyl)amine)2](NO₃)3*3H₂O

Guidance literature:: With NaOH; In water; pH-adjustment of stoich. mixt. of metal salt and ligand to 2.0 (3 M NaOH); crystn. (2 h), collection (filtration), drying (vac.); elem. anal.;
DOI:10.1021/ic971488g