C₁₅H₁₄N₂O

Base Information

Chemical Name:C₁₅H₁₄N₂O
CAS No.:1420830-36-9
Molecular Formula:C₁₅H₁₄N₂O
Molecular Weight:238.289
Hs Code.:

C<sub>15</sub>H<sub>14</sub>N<sub>2</sub>O

Synonyms:C₁₅H₁₄N₂O

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Chemical Property of C₁₅H₁₄N₂O

Chemical Property:

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Technology Process of C₁₅H₁₄N₂O

There total 7 articles about C₁₅H₁₄N₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1420830-35-8
C₁₃H₁₁BrN₂O

: 7486-35-3
tri-n-butyl(vinyl)tin

: 1420830-36-9
C₁₅H₁₄N₂O

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; at 90 ℃; for 1h; under 760.051 Torr; Inert atmosphere;

Reference yield:

: 759-58-0
ethyl isopropylidenecyanoacetate

: 1420830-36-9
C₁₅H₁₄N₂O

Guidance literature:: Multi-step reaction with 6 steps

1.1: ethanol / 6 h / 760.05 Torr / Reflux

2.1: hydrogen bromide; acetic acid / 2 h / 40 - 55 °C / 760.05 Torr

2.2: 760.05 Torr / Cooling with ice

3.1: sodium hydroxide; water / 1,4-dioxane / 12 h / 760.05 Torr / Reflux

3.2: 760.05 Torr / pH 1

4.1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 2 h / 20 °C / 760.05 Torr

5.1: triethylamine / tetrahydrofuran / 1 h / 0 - 20 °C / 760.05 Torr

6.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 1 h / 90 °C / 760.05 Torr / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; oxalyl dichloride; water; hydrogen bromide; acetic acid; triethylamine; N,N-dimethyl-formamide; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 65996-11-4
1-carbethoxy-1-cyano-2-methyl-4-dimethylamino-1,4-butadiene

: 1420830-36-9
C₁₅H₁₄N₂O

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogen bromide; acetic acid / 2 h / 40 - 55 °C / 760.05 Torr

1.2: 760.05 Torr / Cooling with ice

2.1: sodium hydroxide; water / 1,4-dioxane / 12 h / 760.05 Torr / Reflux

2.2: 760.05 Torr / pH 1

3.1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 2 h / 20 °C / 760.05 Torr

4.1: triethylamine / tetrahydrofuran / 1 h / 0 - 20 °C / 760.05 Torr

5.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 1 h / 90 °C / 760.05 Torr / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; oxalyl dichloride; water; hydrogen bromide; acetic acid; triethylamine; N,N-dimethyl-formamide; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;