Diphenyldiisopropylsilan

Base Information

• Chemical Name: Diphenyldiisopropylsilan
• CAS No.: 75544-10-4
• Molecular Formula: C₁₈H₂₄Si
• Molecular Weight: 268.474
• Mol file: 75544-10-4.mol

Synonyms:Diphenyldiisopropylsilan

Chemical Property of Diphenyldiisopropylsilan

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of Diphenyldiisopropylsilan

There total 2 articles about Diphenyldiisopropylsilan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

isopropyllithium (1888-75-1) + diphenylsilyl dichloride (80-10-4) → Diphenyldiisopropylsilan (75544-10-4)

Guidance literature:

In Petroleum ether; for 72h; Heating;

DOI:10.1016/S0022-328X(00)90001-9

Reference yield: 63.0%

2-(diisopropylphenylsilyl)phenyl trifluoromethanesulfonate (1116155-54-4) → 9,9-diisopropyl-9-silafluorene (1116155-67-9) + Diphenyldiisopropylsilan (75544-10-4)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; diethylamine; In N,N-dimethyl acetamide; at 100 ℃; for 95h; Overall yield = 20.9 mg;

DOI:10.1002/asia.201800603

upstream raw materials:

isopropyllithium

diphenylsilyl dichloride

2-(diisopropylphenylsilyl)phenyl trifluoromethanesulfonate