1-phenyl-1-methoxy-2-phenylselenenyl propane dichloride, erythro

Base Information

• Chemical Name: 1-phenyl-1-methoxy-2-phenylselenenyl propane dichloride, erythro
• CAS No.: 116118-00-4
• Molecular Formula: C₁₆H₁₈Cl₂OSe
• Molecular Weight: 376.184
• Mol file: 116118-00-4.mol

Synonyms:1-phenyl-1-methoxy-2-phenylselenenyl propane dichloride, erythro

Chemical Property of 1-phenyl-1-methoxy-2-phenylselenenyl propane dichloride, erythro

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-phenyl-1-methoxy-2-phenylselenenyl propane dichloride, erythro

There total 3 articles about 1-phenyl-1-methoxy-2-phenylselenenyl propane dichloride, erythro which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

1-phenyl-1-methoxy-2-phenylselenenyl propane (74880-71-0,74880-72-1,116117-94-3) → 1-phenyl-1-methoxy-2-phenylselenenyl propane dichloride, erythro (116118-00-4)

Guidance literature:

With sulfuryl dichloride; In tetrachloromethane; for 0.5h; Ambient temperature;

DOI:10.1016/S0040-4020(01)81734-8

Reference yield:

Phenylselenyl chloride (5707-04-0) → 1-phenyl-1-methoxy-2-phenylselenenyl propane dichloride, erythro (116118-00-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 78 percent / 1 h / Ambient temperature

2: 93 percent / SO₂Cl₂ / CCl₄ / 0.5 h / Ambient temperature

With sulfuryl dichloride; In tetrachloromethane;

DOI:10.1016/S0040-4020(01)81734-8

Reference yield:

1-propenylbenzene (873-66-5) → 1-phenyl-1-methoxy-2-phenylselenenyl propane dichloride, erythro (116118-00-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 78 percent / 1 h / Ambient temperature

2: 93 percent / SO₂Cl₂ / CCl₄ / 0.5 h / Ambient temperature

With sulfuryl dichloride; In tetrachloromethane;

DOI:10.1016/S0040-4020(01)81734-8

upstream raw materials:

1-phenyl-1-methoxy-2-phenylselenenyl propane

Phenylselenyl chloride

1-propenylbenzene

Downstream raw materials:

2-phenylpropionaldehyde dimethyl acetal

1-phenyl-1,2-dimethoxy propane, erythro

1-phenyl-1,2-dimethoxy propane, threo

1-phenylallyl methyl ether