methyl 2-[(2-Aminobenzyl)-(4-methoxybenzenesulfonyl)amino]-3-hydroxypropionate

Base Information

Chemical Name:methyl 2-[(2-Aminobenzyl)-(4-methoxybenzenesulfonyl)amino]-3-hydroxypropionate
CAS No.:233754-50-2
Molecular Formula:C₁₈H₂₂N₂O₆S
Molecular Weight:394.448
Hs Code.:

Synonyms:methyl 2-[(2-Aminobenzyl)-(4-methoxybenzenesulfonyl)amino]-3-hydroxypropionate

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Chemical Property of methyl 2-[(2-Aminobenzyl)-(4-methoxybenzenesulfonyl)amino]-3-hydroxypropionate

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Technology Process of methyl 2-[(2-Aminobenzyl)-(4-methoxybenzenesulfonyl)amino]-3-hydroxypropionate

There total 4 articles about methyl 2-[(2-Aminobenzyl)-(4-methoxybenzenesulfonyl)amino]-3-hydroxypropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 233754-49-9
methyl 3-Hydroxy-2-[(4-methoxybenzenesulfonyl)-(2-nitrobenzyl)-amino]propionate

: 233754-50-2
methyl 2-[(2-Aminobenzyl)-(4-methoxybenzenesulfonyl)amino]-3-hydroxypropionate

Guidance literature:: With ammonium formate; palladium 10% on activated carbon; In ethanol; at 20 - 80 ℃;

Reference yield:

: 98-68-0
4-methoxy-phenyl-sulphonyl chloride

: 233754-50-2
methyl 2-[(2-Aminobenzyl)-(4-methoxybenzenesulfonyl)amino]-3-hydroxypropionate

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / CH₂Cl₂

2: NaH / dimethylformamide

3: ammonium formate / 10 percent Pd/C / ethanol

With ammonium formate; sodium hydride; triethylamine; palladium on activated charcoal; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(02)00633-9

Reference yield:

: 85622-74-8
methyl 3-hydroxy-2-(4-methoxybenzenesulfonylamino)propionate

: 233754-50-2
methyl 2-[(2-Aminobenzyl)-(4-methoxybenzenesulfonyl)amino]-3-hydroxypropionate

Guidance literature:: Multi-step reaction with 2 steps

1: NaH / dimethylformamide

2: ammonium formate / 10 percent Pd/C / ethanol

With ammonium formate; sodium hydride; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(02)00633-9