4-n-Hexylcyclohexancarbonsaeurehydrazid

Base Information

• Chemical Name: 4-n-Hexylcyclohexancarbonsaeurehydrazid
• CAS No.: 113423-43-1
• Molecular Formula: C₁₃H₂₆N₂O
• Molecular Weight: 226.362
• Mol file: 113423-43-1.mol

Synonyms:4-n-Hexylcyclohexancarbonsaeurehydrazid

Chemical Property of 4-n-Hexylcyclohexancarbonsaeurehydrazid

Chemical Property:

Purity/Quality:

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Technology Process of 4-n-Hexylcyclohexancarbonsaeurehydrazid

There total 1 articles about 4-n-Hexylcyclohexancarbonsaeurehydrazid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-n-hexylcyclohexanecarboxylic acid (38792-92-6) → 4-n-Hexylcyclohexancarbonsaeurehydrazid (113423-43-1)

Guidance literature:

4-n-hexylcyclohexanecarboxylic acid; With sulfuric acid; In methanol; for 4h; Reflux;

With hydrazine hydrate; In methanol; at 75 ℃; for 0.5h;

DOI:10.1016/j.ejmech.2017.12.011

Reference yield:

5-nitrofurane-2-carboxaldehyde (698-63-5) + 4-n-Hexylcyclohexancarbonsaeurehydrazid (113423-43-1) → 4-penpthyl-N'-[(5-nitrofuran-2-yl)methylene] cyclohexane carbohydrazide

Guidance literature:

With sulfuric acid; acetic acid; In water; at 20 ℃;

DOI:10.1016/j.ejmech.2017.12.011

Reference yield:

4-butylbenzoyl chloride (28788-62-7) + 4-n-Hexylcyclohexancarbonsaeurehydrazid (113423-43-1) → 2-(4-n-Butylphenyl)-5-(trans-4-n-hexylcyclohexyl)-1,3,4-thiadiazol (113423-21-5)

Guidance literature:

With 2.) P₂S₁₀; Multistep reaction; 1.) benzene, pyridine, 2.) benzene, pyridine, 1 h, 50 degC, 6 h, 80 degC;

upstream raw materials:

4-n-hexylcyclohexanecarboxylic acid

Downstream raw materials:

2-(4-n-Butylphenyl)-5-(trans-4-n-hexylcyclohexyl)-1,3,4-thiadiazol

2-(4-Hexyl-cyclohexyl)-5-(4-hexyl-phenyl)-[1,3,4]thiadiazole

2-(4-Dodecyl-phenyl)-5-(4-hexyl-cyclohexyl)-[1,3,4]thiadiazole

2,5-Bis-(4-hexyl-cyclohexyl)-[1,3,4]thiadiazole