5-(4-(N-benzylmethylsulfonamido)phenyl)-N,N-dimethyl-1H-pyrazole-1-sulfonamide

Base Information

Chemical Name:5-(4-(N-benzylmethylsulfonamido)phenyl)-N,N-dimethyl-1H-pyrazole-1-sulfonamide
CAS No.:1627211-38-4
Molecular Formula:C₁₉H₂₂N₄O₄S₂
Molecular Weight:434.54
Hs Code.:

Synonyms:5-(4-(N-benzylmethylsulfonamido)phenyl)-N,N-dimethyl-1H-pyrazole-1-sulfonamide

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Chemical Property of 5-(4-(N-benzylmethylsulfonamido)phenyl)-N,N-dimethyl-1H-pyrazole-1-sulfonamide

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Technology Process of 5-(4-(N-benzylmethylsulfonamido)phenyl)-N,N-dimethyl-1H-pyrazole-1-sulfonamide

There total 2 articles about 5-(4-(N-benzylmethylsulfonamido)phenyl)-N,N-dimethyl-1H-pyrazole-1-sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1627211-34-0
N-benzyl-N-(4-bromophenyl)methanesulfonamide

: 133228-21-4
N,N-dimethyl-1H-pyrazole-1-sulfonamide

: 1627211-38-4
5-(4-(N-benzylmethylsulfonamido)phenyl)-N,N-dimethyl-1H-pyrazole-1-sulfonamide

Guidance literature:: With 2-Ethylhexanoic acid; palladium diacetate; potassium carbonate; triphenylphosphine; In 5,5-dimethyl-1,3-cyclohexadiene; at 20 - 130 ℃; for 21h; Sealed tube; Inert atmosphere;
DOI:10.1002/adsc.201301139

Reference yield:

: 4284-50-8
N-(4-bromophenyl)methanesulfonamide

: 100-44-7
benzyl chloride

: 1627211-38-4
5-(4-(N-benzylmethylsulfonamido)phenyl)-N,N-dimethyl-1H-pyrazole-1-sulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 20 - 60 °C

2: potassium carbonate; triphenylphosphine; palladium diacetate; 2-Ethylhexanoic acid / 5,5-dimethyl-1,3-cyclohexadiene / 21 h / 20 - 130 °C / Sealed tube; Inert atmosphere

With 2-Ethylhexanoic acid; palladium diacetate; potassium carbonate; triphenylphosphine; In 5,5-dimethyl-1,3-cyclohexadiene; N,N-dimethyl-formamide;
DOI:10.1002/adsc.201301139