[1,2,4]triazolo[1.5-a]pyridine-6-carboxylic acid 4-benzenesulfonylbenzylamide

Base Information

Chemical Name:[1,2,4]triazolo[1.5-a]pyridine-6-carboxylic acid 4-benzenesulfonylbenzylamide
CAS No.:1454284-56-0
Molecular Formula:C₂₀H₁₆N₄O₃S
Molecular Weight:392.438
Hs Code.:

Synonyms:[1,2,4]triazolo[1.5-a]pyridine-6-carboxylic acid 4-benzenesulfonylbenzylamide

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Chemical Property of [1,2,4]triazolo[1.5-a]pyridine-6-carboxylic acid 4-benzenesulfonylbenzylamide

Chemical Property:

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Technology Process of [1,2,4]triazolo[1.5-a]pyridine-6-carboxylic acid 4-benzenesulfonylbenzylamide

There total 8 articles about [1,2,4]triazolo[1.5-a]pyridine-6-carboxylic acid 4-benzenesulfonylbenzylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

: 1043903-19-0
[1,2,4]triazolo[1,5-a]pyridine-6-carboxylic acid

: 94341-56-7
[4-(benzenesulfonyl)phenyl]methanamine

: 1454284-56-0
[1,2,4]triazolo[1.5-a]pyridine-6-carboxylic acid 4-benzenesulfonylbenzylamide

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 10h;

Reference yield:

: 1194-02-1,143234-87-1
4-fluorobenzonitrile

: 1454284-56-0
[1,2,4]triazolo[1.5-a]pyridine-6-carboxylic acid 4-benzenesulfonylbenzylamide

Guidance literature:: Multi-step reaction with 3 steps

1: dimethyl sulfoxide / 16 h / 130 °C

2: ammonia; hydrogen / methanol / 16 h / 2585.81 Torr / Inert atmosphere

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; benzotriazol-1-ol / N,N-dimethyl-formamide / 10 h / 20 °C

With ammonia; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In methanol; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 873-55-2
sodium benzenesulfonate

: 1454284-56-0
[1,2,4]triazolo[1.5-a]pyridine-6-carboxylic acid 4-benzenesulfonylbenzylamide

Guidance literature:: Multi-step reaction with 3 steps

1: dimethyl sulfoxide / 16 h / 130 °C

2: ammonia; hydrogen / methanol / 16 h / 2585.81 Torr / Inert atmosphere

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; benzotriazol-1-ol / N,N-dimethyl-formamide / 10 h / 20 °C

With ammonia; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In methanol; dimethyl sulfoxide; N,N-dimethyl-formamide;