5-(bromomethyl)-5-methyl-3-phenyl-4,5-dihydroisoxazole

Base Information

Chemical Name:5-(bromomethyl)-5-methyl-3-phenyl-4,5-dihydroisoxazole
CAS No.:68843-62-9
Molecular Formula:C₁₁H₁₂BrNO
Molecular Weight:254.126
Hs Code.:

Synonyms:5-(bromomethyl)-5-methyl-3-phenyl-4,5-dihydroisoxazole

Suppliers and Price of 5-(bromomethyl)-5-methyl-3-phenyl-4,5-dihydroisoxazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 5-(bromomethyl)-5-methyl-3-phenyl-4,5-dihydroisoxazole

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5-(bromomethyl)-5-methyl-3-phenyl-4,5-dihydroisoxazole

There total 5 articles about 5-(bromomethyl)-5-methyl-3-phenyl-4,5-dihydroisoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 68843-68-5
1-phenyl-3-methyl-but-3-en-1-one oxime

: 68843-62-9
5-(bromomethyl)-5-methyl-3-phenyl-4,5-dihydroisoxazole

Guidance literature:: With palladium diacetate; copper dichloride; In dimethyl sulfoxide; at 20 ℃; for 5h; Inert atmosphere;
DOI:10.1002/ejoc.201403538

Reference yield:

: 100-52-7
benzaldehyde

: 68843-62-9
5-(bromomethyl)-5-methyl-3-phenyl-4,5-dihydroisoxazole

Guidance literature:: Multi-step reaction with 4 steps

1: indium / water; tetrahydrofuran

2: Jones reagent / diethyl ether / 1 h / 0 - 20 °C

3: hydroxylamine hydrochloride; sodium acetate / water; ethanol / 20 °C

4: palladium diacetate; copper dichloride / dimethyl sulfoxide / 5 h / 20 °C / Inert atmosphere

With indium; Jones reagent; hydroxylamine hydrochloride; sodium acetate; palladium diacetate; copper dichloride; In tetrahydrofuran; diethyl ether; ethanol; water; dimethyl sulfoxide;
DOI:10.1002/ejoc.201403538

Reference yield:

: 23092-23-1
3-methyl-1-phenylbut-3-en-1-ol

: 68843-62-9
5-(bromomethyl)-5-methyl-3-phenyl-4,5-dihydroisoxazole

Guidance literature:: Multi-step reaction with 3 steps

1: Jones reagent / diethyl ether / 1 h / 0 - 20 °C

2: hydroxylamine hydrochloride; sodium acetate / water; ethanol / 20 °C

3: palladium diacetate; copper dichloride / dimethyl sulfoxide / 5 h / 20 °C / Inert atmosphere

With Jones reagent; hydroxylamine hydrochloride; sodium acetate; palladium diacetate; copper dichloride; In diethyl ether; ethanol; water; dimethyl sulfoxide;
DOI:10.1002/ejoc.201403538