Technology Process of 4-Pentenoic acid, 5-chloro-2-(1-methylethyl)-, (4E)-
There total 7 articles about 4-Pentenoic acid, 5-chloro-2-(1-methylethyl)-, (4E)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
methyl (4E)-5-chloro-2-isopropyl-4-pentenoate;
With
sodium hydroxide;
In
water;
at 100 - 110 ℃;
for 2h;
under 2250.23 Torr;
With
sulfuric acid; water;
pH=1.5;
Product distribution / selectivity;
- Guidance literature:
-
dimethyl isopropylmalonate;
With
sodium methylate;
In
methanol; N,N-dimethyl-formamide;
at 60 ℃;
With
(E)-1,3-dichloro-prop-1-ene;
at 80 ℃;
for 2.5h;
With
sodium hydroxide; sulfuric acid; water; calcium chloride;
more than 3 stages;
Product distribution / selectivity;
- Guidance literature:
-
With
sodium hydroxide; water;
In
ethanol;
for 18h;
Heating / reflux;