C₅₁H₇₃O₇Si₂N₃NOCH₃

Base Information

Chemical Name:C₅₁H₇₃O₇Si₂N₃NOCH₃
CAS No.:183788-33-2
Molecular Formula:C₅₂H₇₆N₄O₈Si₂
Molecular Weight:941.368
Hs Code.:

C<sub>51</sub>H<sub>73</sub>O<sub>7</sub>Si<sub>2</sub>N<sub>3</sub>NOCH<sub>3</sub>

Synonyms:C₅₁H₇₃O₇Si₂N₃NOCH₃

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Chemical Property of C₅₁H₇₃O₇Si₂N₃NOCH₃

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Technology Process of C₅₁H₇₃O₇Si₂N₃NOCH₃

There total 3 articles about C₅₁H₇₃O₇Si₂N₃NOCH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 593-56-6
N-methoxylamine hydrochloride

: 170510-32-4
C₅₁H₇₃N₃O₈Si₂

: 183788-33-2
C₅₁H₇₃O₇Si₂N₃NOCH₃

Guidance literature:: With pyridine; In dichloromethane; at 0 - 25 ℃; for 4h;
DOI:10.1021/ja972160p

Reference yield:

: 170510-28-8
C₅₁H₇₄O₈Si₂

: 183788-33-2
C₅₁H₇₃O₇Si₂N₃NOCH₃

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / PTAB; HOAc / tetrahydrofuran / 0 °C

2: 100 percent / TMGA / acetonitrile / 6 h

3: 98 percent / pyridine / CH₂Cl₂ / 2 h / 20 °C

With pyridine; PTAB; acetic acid; In tetrahydrofuran; dichloromethane; acetonitrile; 1: Bromination / 2: Substitution / 3: Condensation;
DOI:10.1021/ol991153y

Reference yield:

: C₅₁H₇₃BrO₈Si₂

: 183788-33-2
C₅₁H₇₃O₇Si₂N₃NOCH₃

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / TMGA / acetonitrile / 6 h

2: 98 percent / pyridine / CH₂Cl₂ / 2 h / 20 °C

With pyridine; In dichloromethane; acetonitrile; 1: Substitution / 2: Condensation;
DOI:10.1021/ol991153y