(1R,2'R,3'S)-2,2-dimethyl-(2,3-diphenyl-1-propylaziridin-2-yl)propan-1-ol

Base Information

• Chemical Name: (1R,2'R,3'S)-2,2-dimethyl-(2,3-diphenyl-1-propylaziridin-2-yl)propan-1-ol
• CAS No.: 1268397-03-0
• Molecular Formula: C₂₂H₂₉NO
• Molecular Weight: 323.478

Synonyms:(1R,2'R,3'S)-2,2-dimethyl-(2,3-diphenyl-1-propylaziridin-2-yl)propan-1-ol

Chemical Property of (1R,2'R,3'S)-2,2-dimethyl-(2,3-diphenyl-1-propylaziridin-2-yl)propan-1-ol

Chemical Property:

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Technology Process of (1R,2'R,3'S)-2,2-dimethyl-(2,3-diphenyl-1-propylaziridin-2-yl)propan-1-ol

There total 1 articles about (1R,2'R,3'S)-2,2-dimethyl-(2,3-diphenyl-1-propylaziridin-2-yl)propan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

(S,S)-N-propyl-2,3-diphenylaziridine (1020745-28-1,307310-77-6) + pivalaldehyde (630-19-3) → (1R,2'R,3'S)-2,2-dimethyl-(2,3-diphenyl-1-propylaziridin-2-yl)propan-1-ol (1268397-03-0)

Guidance literature:

(S,S)-N-propyl-2,3-diphenylaziridine; With sec.-butyllithium; In tetrahydrofuran; cyclohexane; at -78 ℃; for 3h; Inert atmosphere;

pivalaldehyde; In tetrahydrofuran; cyclohexane; at -78 ℃; optical yield given as %de; stereoselective reaction; Inert atmosphere;

DOI:10.1002/chem.201002172

Reference yield:

(1R,2'R,3'S)-2,2-dimethyl-(2,3-diphenyl-1-propylaziridin-2-yl)propan-1-ol (1268397-03-0) + R-(+)-α-trifluoromethyl-α-methoxy-phenylacetic acid (20445-31-2) → C10H9F3O3*C22H29NO

Guidance literature:

In chloroform-d1; for 48h;

DOI:10.1002/chem.201002172

upstream raw materials:

(S,S)-N-propyl-2,3-diphenylaziridine

pivalaldehyde

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