C₂₇H₂₅N₃O₄S

Base Information

Chemical Name:C₂₇H₂₅N₃O₄S
CAS No.:1552321-48-8
Molecular Formula:C₂₇H₂₅N₃O₄S
Molecular Weight:487.579
Hs Code.:

C<sub>27</sub>H<sub>25</sub>N<sub>3</sub>O<sub>4</sub>S

Synonyms:C₂₇H₂₅N₃O₄S

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Chemical Property of C₂₇H₂₅N₃O₄S

Chemical Property:

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Technology Process of C₂₇H₂₅N₃O₄S

There total 7 articles about C₂₇H₂₅N₃O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1552320-80-5
ethyl 2-[4-[(2-chloro-5,5-dioxo-7,8-dihydro-6H-thiopyrano[3,2-d]pyrimidin-4-yl)amino]phenyl]acetate

: 32316-92-0
naphthalene-2-boronic acid

: 1552321-48-8
C₂₇H₂₅N₃O₄S

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; sodium carbonate; In 1,2-dimethoxyethane; water; at 130 ℃; for 1h; Microwave irradiation;
DOI:10.1016/j.bmcl.2013.12.076

Reference yield:

: 38555-40-7
methyl 4-{[2-(methyloxy)-2-oxoethyl]thio}butanoate

: 1552321-48-8
C₂₇H₂₅N₃O₄S

Guidance literature:: Multi-step reaction with 7 steps

1: sodium methylate / toluene / 3 h / 105 °C

2: potassium hydroxide / methanol / 16 h / 20 °C

3: water; acetic acid / 72 h / 110 °C

4: N,N-dimethyl-aniline; trichlorophosphate / 18 h / 90 °C

5: N-ethyl-N,N-diisopropylamine / ethanol / 65 h / Reflux

6: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 24 h / 20 °C

7: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; sodium carbonate / 1,2-dimethoxyethane; water / 1 h / 130 °C / Microwave irradiation

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; water; sodium methylate; sodium carbonate; acetic acid; N,N-dimethyl-aniline; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; potassium hydroxide; trichlorophosphate; In methanol; 1,2-dimethoxyethane; ethanol; dichloromethane; water; toluene; 1: |Dieckmann Condensation;
DOI:10.1016/j.bmcl.2013.12.076

Reference yield:

: 38555-41-8
methyl 3-oxo-2,3,4,5-tetrahydro-6H-thiopyran-2-carboxylate

: 1552321-48-8
C₂₇H₂₅N₃O₄S

Guidance literature:: Multi-step reaction with 6 steps

1: potassium hydroxide / methanol / 16 h / 20 °C

2: water; acetic acid / 72 h / 110 °C

3: N,N-dimethyl-aniline; trichlorophosphate / 18 h / 90 °C

4: N-ethyl-N,N-diisopropylamine / ethanol / 65 h / Reflux

5: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 24 h / 20 °C

6: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; sodium carbonate / 1,2-dimethoxyethane; water / 1 h / 130 °C / Microwave irradiation

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; water; sodium carbonate; acetic acid; N,N-dimethyl-aniline; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; potassium hydroxide; trichlorophosphate; In methanol; 1,2-dimethoxyethane; ethanol; dichloromethane; water;
DOI:10.1016/j.bmcl.2013.12.076