Technology Process of C30H24FN3O5S
There total 7 articles about C30H24FN3O5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
acetone;
for 1.5h;
Cooling with ice;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: tetrahydrofuran / 1 h / Cooling with ice
2.1: sodium hydroxide; water / methanol / 0.5 h / Cooling with ice
3.1: sulfuric acid / 4 h / Cooling with ice
4.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 3 h / 20 °C
5.1: borane-THF / tetrahydrofuran / 3 h / 20 °C / Cooling with ice
5.2: 0.25 h / 20 °C / Cooling with ice
6.1: acetone / 1.5 h / Cooling with ice
With
borane-THF; oxalyl dichloride; sulfuric acid; water; sodium hydroxide;
N,N-dimethyl-formamide;
In
tetrahydrofuran; methanol; dichloromethane; acetone;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: tetrahydrofuran / 1 h / Cooling with ice
2.1: sodium hydroxide; water / methanol / 0.5 h / Cooling with ice
3.1: sulfuric acid / 4 h / Cooling with ice
4.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 3 h / 20 °C
5.1: borane-THF / tetrahydrofuran / 3 h / 20 °C / Cooling with ice
5.2: 0.25 h / 20 °C / Cooling with ice
6.1: acetone / 1.5 h / Cooling with ice
With
borane-THF; oxalyl dichloride; sulfuric acid; water; sodium hydroxide;
N,N-dimethyl-formamide;
In
tetrahydrofuran; methanol; dichloromethane; acetone;