2-(1-(phenylsulfonyl)indol-2-yl)-2-oxoethanal

Base Information

Chemical Name:2-(1-(phenylsulfonyl)indol-2-yl)-2-oxoethanal
CAS No.:117966-23-1
Molecular Formula:C₁₆H₁₁NO₄S
Molecular Weight:313.334
Hs Code.:

Synonyms:2-(1-(phenylsulfonyl)indol-2-yl)-2-oxoethanal

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Chemical Property of 2-(1-(phenylsulfonyl)indol-2-yl)-2-oxoethanal

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Technology Process of 2-(1-(phenylsulfonyl)indol-2-yl)-2-oxoethanal

There total 5 articles about 2-(1-(phenylsulfonyl)indol-2-yl)-2-oxoethanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 120-72-9
indole

: 117966-23-1
2-(1-(phenylsulfonyl)indol-2-yl)-2-oxoethanal

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) n-BuLi

2: 1.) LDA

3: 90 percent / activated MnO₂ / CHCl₃ / 18 h / Heating

4: 1.) SeO₂, H₂O / 1.) dioxane, reflux, 1 h, 2.) dioxane, reflux, 12 h

With manganese(IV) oxide; n-butyllithium; selenium(IV) oxide; water; lithium diisopropyl amide; In chloroform;
DOI:10.1016/S0040-4020(01)85951-2

Reference yield:

: 40899-71-6
1-benzenesulfonylindole

: 117966-23-1
2-(1-(phenylsulfonyl)indol-2-yl)-2-oxoethanal

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) LDA

2: 90 percent / activated MnO₂ / CHCl₃ / 18 h / Heating

3: 1.) SeO₂, H₂O / 1.) dioxane, reflux, 1 h, 2.) dioxane, reflux, 12 h

With manganese(IV) oxide; selenium(IV) oxide; water; lithium diisopropyl amide; In chloroform;
DOI:10.1016/S0040-4020(01)85951-2

Reference yield:

: 80360-24-3
1<1-(phenylsulfonyl)indol-2-yl>ethanol

: 117966-23-1
2-(1-(phenylsulfonyl)indol-2-yl)-2-oxoethanal

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / activated MnO₂ / CHCl₃ / 18 h / Heating

2: 1.) SeO₂, H₂O / 1.) dioxane, reflux, 1 h, 2.) dioxane, reflux, 12 h

With manganese(IV) oxide; selenium(IV) oxide; water; In chloroform;
DOI:10.1016/S0040-4020(01)85951-2