cis-4-(4'-methoxyphenyl)-3-phenoxy-1-(2'-phenyl-2'-trimethylsiloxyethyl)azetidin-2-one

Base Information

Chemical Name:cis-4-(4'-methoxyphenyl)-3-phenoxy-1-(2'-phenyl-2'-trimethylsiloxyethyl)azetidin-2-one
CAS No.:102488-26-6
Molecular Formula:C₂₇H₃₁NO₄Si
Molecular Weight:461.633
Hs Code.:

Synonyms:cis-4-(4'-methoxyphenyl)-3-phenoxy-1-(2'-phenyl-2'-trimethylsiloxyethyl)azetidin-2-one

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Chemical Property of cis-4-(4'-methoxyphenyl)-3-phenoxy-1-(2'-phenyl-2'-trimethylsiloxyethyl)azetidin-2-one

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Technology Process of cis-4-(4'-methoxyphenyl)-3-phenoxy-1-(2'-phenyl-2'-trimethylsiloxyethyl)azetidin-2-one

There total 4 articles about cis-4-(4'-methoxyphenyl)-3-phenoxy-1-(2'-phenyl-2'-trimethylsiloxyethyl)azetidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 93681-46-0
[1-(4-Methoxy-phenyl)-meth-(E)-ylidene]-(2-phenyl-2-trimethylsilanyloxy-ethyl)-amine

: 122-59-8
2-phenoxyacetic acid

: 102488-26-6
cis-4-(4'-methoxyphenyl)-3-phenoxy-1-(2'-phenyl-2'-trimethylsiloxyethyl)azetidin-2-one

Guidance literature:: With thionyl chloride; triethylamine; N,N-dimethyl-formamide; In dichloromethane; benzene; Ambient temperature;

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 102488-26-6
cis-4-(4'-methoxyphenyl)-3-phenoxy-1-(2'-phenyl-2'-trimethylsiloxyethyl)azetidin-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: MgSO₄ / CH₂Cl₂ / 2 h / Ambient temperature

2: Et₃N / CH₂Cl₂ / 1 h / Ambient temperature

3: 30 percent / DMF-SOCl₂, Et₃N / benzene; CH₂Cl₂ / Ambient temperature

With thionyl chloride; magnesium sulfate; triethylamine; N,N-dimethyl-formamide; In dichloromethane; benzene;

Reference yield:

: 93681-42-6
2-{[1-(4-Methoxy-phenyl)-meth-(E)-ylidene]-amino}-1-phenyl-ethanol

: 102488-26-6
cis-4-(4'-methoxyphenyl)-3-phenoxy-1-(2'-phenyl-2'-trimethylsiloxyethyl)azetidin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / 1 h / Ambient temperature

2: 30 percent / DMF-SOCl₂, Et₃N / benzene; CH₂Cl₂ / Ambient temperature

With thionyl chloride; triethylamine; N,N-dimethyl-formamide; In dichloromethane; benzene;