Welcome to LookChem.com Sign In|Join Free
  • or

Encyclopedia

<1R-(1β,2α,3α,4β)>-2,3-(dimethylmethylenedioxy)-4-<(phenylmethoxy)methyl>-1-cyclopentanamine hydriodide

Base Information Edit
  • Chemical Name:<1R-(1β,2α,3α,4β)>-2,3-(dimethylmethylenedioxy)-4-<(phenylmethoxy)methyl>-1-cyclopentanamine hydriodide
  • CAS No.:100021-28-1
  • Molecular Formula:C16H23NO3*HI
  • Molecular Weight:405.276
  • Hs Code.:
  • Mol file:100021-28-1.mol
<1R-(1β,2α,3α,4β)>-2,3-(dimethylmethylenedioxy)-4-<(phenylmethoxy)methyl>-1-cyclopentanamine hydriodide

Synonyms:<1R-(1β,2α,3α,4β)>-2,3-(dimethylmethylenedioxy)-4-<(phenylmethoxy)methyl>-1-cyclopentanamine hydriodide

Suppliers and Price of <1R-(1β,2α,3α,4β)>-2,3-(dimethylmethylenedioxy)-4-<(phenylmethoxy)methyl>-1-cyclopentanamine hydriodide
Supply Marketing:Edit
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
Manufacturers and distributors:
  • Manufacture/Brand
  • Chemicals and raw materials
  • Packaging
  • price
Total 0 raw suppliers
Chemical Property of <1R-(1β,2α,3α,4β)>-2,3-(dimethylmethylenedioxy)-4-<(phenylmethoxy)methyl>-1-cyclopentanamine hydriodide Edit
Chemical Property:
Purity/Quality:
Safty Information:
  • Pictogram(s):  
  • Hazard Codes: 
MSDS Files:
Useful:
Technology Process of <1R-(1β,2α,3α,4β)>-2,3-(dimethylmethylenedioxy)-4-<(phenylmethoxy)methyl>-1-cyclopentanamine hydriodide

There total 9 articles about <1R-(1β,2α,3α,4β)>-2,3-(dimethylmethylenedioxy)-4-<(phenylmethoxy)methyl>-1-cyclopentanamine hydriodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 9 steps
1: O2, thiourea, sodium acetate, Rose bengal / methanol / 9 h / -5 °C / Irradiation
2: 62 percent / m-chloroperoxybenzoic acid / CH2Cl2 / 48 h / Ambient temperature
3: 100 percent / sodium azide / dimethylformamide / 12 h / 110 °C
4: 92 percent / 75percent aq. HClO4 / acetone / 1 h / Ambient temperature
5: pyridine, 4-(dimethylamino)pyridine / CH2Cl2 / 2 h / Ambient temperature
6: 91 percent / NaOH / tetrahydrofuran / 4 h / Heating
7: pyridine / CH2Cl2 / 2 h / Ambient temperature
8: LiI / dimethylformamide / 1 h / Ambient temperature
9: 55 percent / H2 / 10percent Pd/C / methanol / 6 h / 1034.3 Torr / Ambient temperature
With pyridine; dmap; sodium hydroxide; sodium azide; perchloric acid; hydrogen; oxygen; sodium acetate; rose bengal; thiourea; 3-chloro-benzenecarboperoxoic acid; lithium iodide; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetone;
DOI:10.1021/jo00358a023
Guidance literature:
Multi-step reaction with 8 steps
1: 62 percent / m-chloroperoxybenzoic acid / CH2Cl2 / 48 h / Ambient temperature
2: 100 percent / sodium azide / dimethylformamide / 12 h / 110 °C
3: 92 percent / 75percent aq. HClO4 / acetone / 1 h / Ambient temperature
4: pyridine, 4-(dimethylamino)pyridine / CH2Cl2 / 2 h / Ambient temperature
5: 91 percent / NaOH / tetrahydrofuran / 4 h / Heating
6: pyridine / CH2Cl2 / 2 h / Ambient temperature
7: LiI / dimethylformamide / 1 h / Ambient temperature
8: 55 percent / H2 / 10percent Pd/C / methanol / 6 h / 1034.3 Torr / Ambient temperature
With pyridine; dmap; sodium hydroxide; sodium azide; perchloric acid; hydrogen; 3-chloro-benzenecarboperoxoic acid; lithium iodide; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetone;
DOI:10.1021/jo00358a023
Refernces Edit
Post RFQ for Price