(R)-S-ethyl hydroxy-phenyl-thioacetate

Base Information

Chemical Name:(R)-S-ethyl hydroxy-phenyl-thioacetate
CAS No.:157982-31-5
Molecular Formula:C₁₀H₁₂O₂S
Molecular Weight:196.27
Hs Code.:

Synonyms:(R)-S-ethyl hydroxy-phenyl-thioacetate

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Chemical Property of (R)-S-ethyl hydroxy-phenyl-thioacetate

Chemical Property:

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Technology Process of (R)-S-ethyl hydroxy-phenyl-thioacetate

There total 5 articles about (R)-S-ethyl hydroxy-phenyl-thioacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 157982-28-0
(1R)-S-ethyl [1-phenyl-1-tetrahydropyran-(2RS)-2-yloxy]-thioacetate

: 157982-31-5
(R)-S-ethyl hydroxy-phenyl-thioacetate

Guidance literature:: With pyridinium p-toluenesulfonate; In ethanol; at 60 ℃; for 6h;
DOI:10.1016/S0040-4020(97)01010-7

Reference yield: 48.0%

: 82027-28-9
S-ethyl 2-hydroxy-2-phenylethanethioate

: 63571-96-0
S-ethyl 2-oxo-2-phenylethanethioate

: 157982-31-5
(R)-S-ethyl hydroxy-phenyl-thioacetate

Guidance literature:: With oxygen; chiral vanadium(V); In toluene; at 20 ℃; for 6h;
DOI:10.1021/jo070575f

Reference yield:

: 100-52-7
benzaldehyde

: 157982-31-5
(R)-S-ethyl hydroxy-phenyl-thioacetate

Guidance literature:: Multi-step reaction with 4 steps

1: 84 percent / NaHMDS, pyridine / tetrahydrofuran

2: 94 percent / TsOH / CH₂Cl₂

3: 1.) trifluoroacetic anhydride, pyridine, 2.) aq. LiOH / 1.) CH₂Cl₂, 0 deg C, 15 min, 2.) THF, from 0 deg C to RT

4: ethanolic PPTS

With pyridine; lithium hydroxide; sodium hexamethyldisilazane; pyridinium p-toluenesulfonate; toluene-4-sulfonic acid; trifluoroacetic anhydride; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c39940001653