methyl 2-benzyloxycarbonylamino-2-deoxy-4-O-mesyl-3-O-methoxycarbonyl-α-D-glucopyranoside

Base Information

Chemical Name:methyl 2-benzyloxycarbonylamino-2-deoxy-4-O-mesyl-3-O-methoxycarbonyl-α-D-glucopyranoside
CAS No.:1350556-10-3
Molecular Formula:C₁₈H₂₅NO₁₁S
Molecular Weight:463.463
Hs Code.:

Synonyms:methyl 2-benzyloxycarbonylamino-2-deoxy-4-O-mesyl-3-O-methoxycarbonyl-α-D-glucopyranoside

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Chemical Property of methyl 2-benzyloxycarbonylamino-2-deoxy-4-O-mesyl-3-O-methoxycarbonyl-α-D-glucopyranoside

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Technology Process of methyl 2-benzyloxycarbonylamino-2-deoxy-4-O-mesyl-3-O-methoxycarbonyl-α-D-glucopyranoside

There total 9 articles about methyl 2-benzyloxycarbonylamino-2-deoxy-4-O-mesyl-3-O-methoxycarbonyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1350556-13-6
methyl 2-benzyloxycarbonylamino-2-deoxy-4-O-mesyl-3-O-methoxycarbonyl-6-O-tert-butyldimethylsilyl-α-D-glucopyranoside

: 1350556-10-3
methyl 2-benzyloxycarbonylamino-2-deoxy-4-O-mesyl-3-O-methoxycarbonyl-α-D-glucopyranoside

Guidance literature:: With tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1021/ol2027703

Reference yield:

: 1350556-11-4
methyl 2-benzyloxycarbonylamino-2-deoxy-3-O-methoxycarbonyl-6-O-tert-butyldimethylsilyl-α-D-glucopyranoside

: 1350556-10-3
methyl 2-benzyloxycarbonylamino-2-deoxy-4-O-mesyl-3-O-methoxycarbonyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 3 h / 20 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere

With tetrabutyl ammonium fluoride; acetic acid; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol2027703

Reference yield:

: methyl 4,6-O-benzylidene-2-benzyloxycarbonylamino-2-deoxy-3-O-methoxycarbonyl-α-D-glucopyranoside

: 1350556-10-3
methyl 2-benzyloxycarbonylamino-2-deoxy-4-O-mesyl-3-O-methoxycarbonyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: acetic acid / dichloromethane / 16 h / 60 °C / Inert atmosphere

2: dmap; triethylamine / dichloromethane / 16 h / 0 - 20 °C / Inert atmosphere

3: triethylamine / dichloromethane / 3 h / 20 °C / Inert atmosphere

4: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere

With dmap; tetrabutyl ammonium fluoride; acetic acid; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol2027703