methyl 2-benzyloxycarbonylamino-2-deoxy-3-O-methoxycarbonyl-α-D-glucopyranoside

Base Information

Chemical Name:methyl 2-benzyloxycarbonylamino-2-deoxy-3-O-methoxycarbonyl-α-D-glucopyranoside
CAS No.:1350556-07-8
Molecular Formula:C₁₇H₂₃NO₉
Molecular Weight:385.371
Hs Code.:

Synonyms:methyl 2-benzyloxycarbonylamino-2-deoxy-3-O-methoxycarbonyl-α-D-glucopyranoside

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Chemical Property of methyl 2-benzyloxycarbonylamino-2-deoxy-3-O-methoxycarbonyl-α-D-glucopyranoside

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Technology Process of methyl 2-benzyloxycarbonylamino-2-deoxy-3-O-methoxycarbonyl-α-D-glucopyranoside

There total 6 articles about methyl 2-benzyloxycarbonylamino-2-deoxy-3-O-methoxycarbonyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: methyl 4,6-O-benzylidene-2-benzyloxycarbonylamino-2-deoxy-3-O-methoxycarbonyl-α-D-glucopyranoside

: 1350556-07-8
methyl 2-benzyloxycarbonylamino-2-deoxy-3-O-methoxycarbonyl-α-D-glucopyranoside

Guidance literature:: With acetic acid; In dichloromethane; at 60 ℃; for 16h; Inert atmosphere;
DOI:10.1021/ol2027703

Reference yield:

: 60076-41-7
methyl 4,6-O-benzylidene-2-(benzyloxycarbonyl)amino-2-deoxy-α-D-glucopyranoside

: 1350556-07-8
methyl 2-benzyloxycarbonylamino-2-deoxy-3-O-methoxycarbonyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 1 h / 0 - 20 °C / Inert atmosphere

2: acetic acid / dichloromethane / 16 h / 60 °C / Inert atmosphere

With pyridine; acetic acid; In dichloromethane;
DOI:10.1021/ol2027703

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 1350556-07-8
methyl 2-benzyloxycarbonylamino-2-deoxy-3-O-methoxycarbonyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydrogencarbonate / water / Inert atmosphere

2: acetyl chloride / 24 h / 20 °C / Inert atmosphere

3: formic acid / 24 h / 20 °C / Inert atmosphere

4: pyridine / 1 h / 0 - 20 °C / Inert atmosphere

5: acetic acid / dichloromethane / 16 h / 60 °C / Inert atmosphere

With pyridine; formic acid; sodium hydrogencarbonate; acetic acid; acetyl chloride; In dichloromethane; water;
DOI:10.1021/ol2027703