Technology Process of 1-(naphthalen-2-yl)-1,3-diphenylurea
There total 5 articles about 1-(naphthalen-2-yl)-1,3-diphenylurea which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C17H12N2;
With
acetic acid;
In
toluene;
for 0.5h;
Inert atmosphere;
diphenyliodonium hexafluorophosphate;
With
copper(II) bis(trifluoromethanesulfonate);
In
water; toluene;
at 60 ℃;
for 21h;
Inert atmosphere;
DOI:10.1021/jo501334u
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: caesium carbonate / toluene / 5 h / 20 °C / Inert atmosphere
2.1: acetic acid / toluene / 0.5 h / Inert atmosphere
2.2: 21 h / 60 °C / Inert atmosphere
With
caesium carbonate; acetic acid;
In
toluene;
DOI:10.1021/jo501334u
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydrogencarbonate / toluene / 3 h / 20 °C / Inert atmosphere
2.1: caesium carbonate / toluene / 5 h / 20 °C / Inert atmosphere
3.1: acetic acid / toluene / 0.5 h / Inert atmosphere
3.2: 21 h / 60 °C / Inert atmosphere
With
sodium hydrogencarbonate; caesium carbonate; acetic acid;
In
toluene;
DOI:10.1021/jo501334u
