c[Lys-Lys(1-(4,4-dimethyl-2,6-dioxocyclohex-1-ylidene)-3-methylbutyl)-Leu-Lys-Lys(CO-C₅H₁₁)-Phe-Lys-Lys-Leu-Gln]

Base Information

• Chemical Name: c[Lys-Lys(1-(4,4-dimethyl-2,6-dioxocyclohex-1-ylidene)-3-methylbutyl)-Leu-Lys-Lys(CO-C₅H₁₁)-Phe-Lys-Lys-Leu-Gln]
• CAS No.: 1622984-06-8
• Molecular Formula: C₈₁H₁₃₉N₁₇O₁₄
• Molecular Weight: 1575.1

Synonyms:c[Lys-Lys(1-(4,4-dimethyl-2,6-dioxocyclohex-1-ylidene)-3-methylbutyl)-Leu-Lys-Lys(CO-C₅H₁₁)-Phe-Lys-Lys-Leu-Gln]

Chemical Property of c[Lys-Lys(1-(4,4-dimethyl-2,6-dioxocyclohex-1-ylidene)-3-methylbutyl)-Leu-Lys-Lys(CO-C₅H₁₁)-Phe-Lys-Lys-Leu-Gln]

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Technology Process of c[Lys-Lys(1-(4,4-dimethyl-2,6-dioxocyclohex-1-ylidene)-3-methylbutyl)-Leu-Lys-Lys(CO-C₅H₁₁)-Phe-Lys-Lys-Leu-Gln]

There total 1 articles about c[Lys-Lys(1-(4,4-dimethyl-2,6-dioxocyclohex-1-ylidene)-3-methylbutyl)-Leu-Lys-Lys(CO-C₅H₁₁)-Phe-Lys-Lys-Leu-Gln] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Fmoc-Leu-OH (35661-60-0) + N-Fmoc L-Phe (35661-40-6) + Fmoc-Lys(tert-butoxycarbonyl) (71989-26-9) + Nα-(9-fluorenylmethoxycarbonyl)-L-glutamic acid α-allyl ester (144120-54-7) + hexanoic acid (142-62-1) + Fmoc-Lys(ivDde)-OH (204777-78-6) + Nα-(9-fluorenylmethoxycarbonyl)-Nε-(2-nitrobenzyloxycarbonyl)-lysine (174653-61-3) → c[Lys-Lys(1-(4,4-dimethyl-2,6-dioxocyclohex-1-ylidene)-3-methylbutyl)-Leu-Lys-Lys(CO-C5H11)-Phe-Lys-Lys-Leu-Gln] (1622984-06-8)

Guidance literature:

Nα-(9-fluorenylmethoxycarbonyl)-L-glutamic acid α-allyl ester; With ethyl cyanoglyoxylate-2-oxime; diisopropyl-carbodiimide; In N,N-dimethyl-formamide;

With piperidine; In N,N-dimethyl-formamide;

Fmoc-Leu-OH; N-Fmoc L-Phe; Fmoc-Lys(tert-butoxycarbonyl); hexanoic acid; Fmoc-Lys(ivDde)-OH; N_α-(9-fluorenylmethoxycarbonyl)-N_ε-(2-nitrobenzyloxycarbonyl)-lysine; Further stages;

DOI:10.1002/ejoc.201402111

upstream raw materials:

Fmoc-Leu-OH

N-Fmoc L-Phe

Fmoc-Lys(tert-butoxycarbonyl)

Nα-(9-fluorenylmethoxycarbonyl)-L-glutamic acid α-allyl ester

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