N-(2-cyanobenzo[d]thiazol-6-yl)-3-methyl-3-(2,4,5-trimethyl-3,6-dioxocyclohexa-1,4-dien-1-yl)butanamide

Base Information

Chemical Name:N-(2-cyanobenzo[d]thiazol-6-yl)-3-methyl-3-(2,4,5-trimethyl-3,6-dioxocyclohexa-1,4-dien-1-yl)butanamide
CAS No.:1426551-41-8
Molecular Formula:C₂₂H₂₁N₃O₃S
Molecular Weight:407.493
Hs Code.:

Synonyms:N-(2-cyanobenzo[d]thiazol-6-yl)-3-methyl-3-(2,4,5-trimethyl-3,6-dioxocyclohexa-1,4-dien-1-yl)butanamide

Suppliers and Price of N-(2-cyanobenzo[d]thiazol-6-yl)-3-methyl-3-(2,4,5-trimethyl-3,6-dioxocyclohexa-1,4-dien-1-yl)butanamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2-cyanobenzo[d]thiazol-6-yl)-3-methyl-3-(2,4,5-trimethyl-3,6-dioxocyclohexa-1,4-dien-1-yl)butanamide

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of N-(2-cyanobenzo[d]thiazol-6-yl)-3-methyl-3-(2,4,5-trimethyl-3,6-dioxocyclohexa-1,4-dien-1-yl)butanamide

There total 4 articles about N-(2-cyanobenzo[d]thiazol-6-yl)-3-methyl-3-(2,4,5-trimethyl-3,6-dioxocyclohexa-1,4-dien-1-yl)butanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

: 7724-12-1
2-cyano-6-aminobenzothiazole

: 40662-29-1
3-methyl-3-(2,4,5-trimethyl-3,6-dioxo-cyclohexa-1,4-dienyl)-butyric acid

: 1426551-41-8
N-(2-cyanobenzo[d]thiazol-6-yl)-3-methyl-3-(2,4,5-trimethyl-3,6-dioxocyclohexa-1,4-dien-1-yl)butanamide

Guidance literature:: 3-methyl-3-(2,4,5-trimethyl-3,6-dioxo-cyclohexa-1,4-dienyl)-butyric acid; With 4-methyl-morpholine; isobutyl chloroformate; In tetrahydrofuran; at 0 ℃; for 0.5h;

2-cyano-6-aminobenzothiazole; In tetrahydrofuran;

Reference yield:

: 700-13-0
Trimethylhydroquinone

: 1426551-41-8
N-(2-cyanobenzo[d]thiazol-6-yl)-3-methyl-3-(2,4,5-trimethyl-3,6-dioxocyclohexa-1,4-dien-1-yl)butanamide

Guidance literature:: Multi-step reaction with 3 steps

1: methanesulfonic acid / 2 h / 70 °C

2: N-Bromosuccinimide; water / acetonitrile; acetone / 0.5 h / 20 °C

3: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / 0.5 h / 0 °C

With 4-methyl-morpholine; N-Bromosuccinimide; methanesulfonic acid; water; isobutyl chloroformate; In tetrahydrofuran; acetone; acetonitrile;

Reference yield:

: 924-50-5
Methyl 3,3-dimethylacrylate

: 1426551-41-8
N-(2-cyanobenzo[d]thiazol-6-yl)-3-methyl-3-(2,4,5-trimethyl-3,6-dioxocyclohexa-1,4-dien-1-yl)butanamide

Guidance literature:: Multi-step reaction with 3 steps

1: methanesulfonic acid / 2 h / 70 °C

2: N-Bromosuccinimide; water / acetonitrile; acetone / 0.5 h / 20 °C

3: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / 0.5 h / 0 °C

With 4-methyl-morpholine; N-Bromosuccinimide; methanesulfonic acid; water; isobutyl chloroformate; In tetrahydrofuran; acetone; acetonitrile;