*,R^*)>-1,1-dimethylethyl N,N-bis<4-methyl-2-<<(phenylmethoxy)carbonyl>amino>pentyl>glycinate

Base Information

• Chemical Name: *,R^*)>-1,1-dimethylethyl N,N-bis<4-methyl-2-<<(phenylmethoxy)carbonyl>amino>pentyl>glycinate
• CAS No.: 101250-57-1
• Molecular Formula: C₃₄H₅₁N₃O₆
• Molecular Weight: 597.795

Synonyms:*,R^*)>-1,1-dimethylethyl N,N-bis<4-methyl-2-<<(phenylmethoxy)carbonyl>amino>pentyl>glycinate

Chemical Property of *,R^*)>-1,1-dimethylethyl N,N-bis<4-methyl-2-<<(phenylmethoxy)carbonyl>amino>pentyl>glycinate

Chemical Property:

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Technology Process of *,R^*)>-1,1-dimethylethyl N,N-bis<4-methyl-2-<<(phenylmethoxy)carbonyl>amino>pentyl>glycinate

There total 1 articles about *,R^*)>-1,1-dimethylethyl N,N-bis<4-methyl-2-<<(phenylmethoxy)carbonyl>amino>pentyl>glycinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Glycine tert-butyl ester (6456-74-2) + (S)-phenylmethyl 2-(2-methylpropyl)-1-aziridinecarboxylate (101250-56-0) → ((S)-2-Benzyloxycarbonylamino-4-methyl-pentylamino)-acetic acid tert-butyl ester (101250-58-2) + *,R*)>-1,1-dimethylethyl N,N-bis<4-methyl-2-<<(phenylmethoxy)carbonyl>amino>pentyl>glycinate (101250-57-1)

Guidance literature:

In ethanol; for 48h; Heating;

DOI:10.1021/jm00156a012

Reference yield:

*,R*)>-1,1-dimethylethyl N,N-bis<4-methyl-2-<<(phenylmethoxy)carbonyl>amino>pentyl>glycinate (101250-57-1) → <2S-<2R*,4*,(R*)>>>-phenylmethyl 2-<<<3-methyl-1-<<3-(2-methylpropyl)-5-oxo-1-piperazinyl>methyl>butyl>amino>carbonyl>-1-pyrrolidinecarboxylate (101399-25-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 89 percent / H₂ / 20percent Pd/C / methanol

2: 1H-benzotriazol-1-ol (HOBT), DCC / tetrahydrofuran

With hydrogen; benzotriazol-1-ol; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; methanol;

DOI:10.1021/jm00156a012

upstream raw materials:

Glycine tert-butyl ester

(S)-phenylmethyl 2-(2-methylpropyl)-1-aziridinecarboxylate

Downstream raw materials:

<2S-<2R^*,4*,(R^*)>>>-phenylmethyl 2-<<<3-methyl-1-<<3-(2-methylpropyl)-5-oxo-1-piperazinyl>methyl>butyl>amino>carbonyl>-1-pyrrolidinecarboxylate

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