5-methoxy-1-<2-methyl-3-oxocyclohex-1-enyl(phenylsulphinyl)methyl>-1,2-dihydrocyclobutabenzene

Base Information

Chemical Name:5-methoxy-1-<2-methyl-3-oxocyclohex-1-enyl(phenylsulphinyl)methyl>-1,2-dihydrocyclobutabenzene
CAS No.:83637-53-0
Molecular Formula:C₂₃H₂₄O₃S
Molecular Weight:380.508
Hs Code.:

Synonyms:5-methoxy-1-<2-methyl-3-oxocyclohex-1-enyl(phenylsulphinyl)methyl>-1,2-dihydrocyclobutabenzene

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Chemical Property of 5-methoxy-1-<2-methyl-3-oxocyclohex-1-enyl(phenylsulphinyl)methyl>-1,2-dihydrocyclobutabenzene

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Technology Process of 5-methoxy-1-<2-methyl-3-oxocyclohex-1-enyl(phenylsulphinyl)methyl>-1,2-dihydrocyclobutabenzene

There total 8 articles about 5-methoxy-1-<2-methyl-3-oxocyclohex-1-enyl(phenylsulphinyl)methyl>-1,2-dihydrocyclobutabenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 83637-52-9
1-<1-hydroxy-2-methylcyclohex-2-enyl(phenylsulphinyl)methyl>-5-methoxy-1,2-dihydrocyclobutabenzene

: 83637-53-0
5-methoxy-1-<2-methyl-3-oxocyclohex-1-enyl(phenylsulphinyl)methyl>-1,2-dihydrocyclobutabenzene

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; for 12h; Ambient temperature;

Reference yield:

: 30267-36-8
5-methoxybenzocyclobuten-1-yl toluene-p-sulphonate

: 83637-53-0
5-methoxy-1-<2-methyl-3-oxocyclohex-1-enyl(phenylsulphinyl)methyl>-1,2-dihydrocyclobutabenzene

Guidance literature:: Multi-step reaction with 4 steps

1: dimethylformamide

2: m-chloroperbenzoic acid / CH₂Cl₂

3: 38 percent / lithium di-isopropylamide / tetrahydrofuran

4: pyridinium chlorochromate / CH₂Cl₂

With 3-chloro-benzenecarboperoxoic acid; pyridinium chlorochromate; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c39820000699

Reference yield:

: 83637-51-8
5-methoxybenzocyclobut-1-enylmethyl phenyl sulphoxide

: 83637-53-0
5-methoxy-1-<2-methyl-3-oxocyclohex-1-enyl(phenylsulphinyl)methyl>-1,2-dihydrocyclobutabenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 38 percent / lithium di-isopropylamide / tetrahydrofuran

2: pyridinium chlorochromate / CH₂Cl₂

With pyridinium chlorochromate; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c39820000699