1-bromo-4-[3-(4-bromophenyl)-1-(1,1-dimethylethyl)-3-phenylpropa-1,2-dienyl]benzene

Base Information

Chemical Name:1-bromo-4-[3-(4-bromophenyl)-1-(1,1-dimethylethyl)-3-phenylpropa-1,2-dienyl]benzene
CAS No.:861721-84-8
Molecular Formula:C₂₅H₂₂Br₂
Molecular Weight:482.258
Hs Code.:

Synonyms:1-bromo-4-[3-(4-bromophenyl)-1-(1,1-dimethylethyl)-3-phenylpropa-1,2-dienyl]benzene

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Chemical Property of 1-bromo-4-[3-(4-bromophenyl)-1-(1,1-dimethylethyl)-3-phenylpropa-1,2-dienyl]benzene

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Technology Process of 1-bromo-4-[3-(4-bromophenyl)-1-(1,1-dimethylethyl)-3-phenylpropa-1,2-dienyl]benzene

There total 6 articles about 1-bromo-4-[3-(4-bromophenyl)-1-(1,1-dimethylethyl)-3-phenylpropa-1,2-dienyl]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 861721-95-1
acetic acid 1,3-bis-(4-bromo-phenyl)-1-phenyl-prop-2-ynyl ester

: 677-22-5
tert-butylmagnesium chloride

: 861721-84-8
1-bromo-4-[3-(4-bromophenyl)-1-(1,1-dimethylethyl)-3-phenylpropa-1,2-dienyl]benzene

Guidance literature:: With copper(l) iodide; lithium bromide; In tetrahydrofuran; diethyl ether; at 0 ℃; for 0.666667h;
DOI:10.1002/ejoc.200500096

Reference yield:

: 861721-94-0
1,3-bis(4-bromophenyl)prop-2-yn-1-ol

: 861721-84-8
1-bromo-4-[3-(4-bromophenyl)-1-(1,1-dimethylethyl)-3-phenylpropa-1,2-dienyl]benzene

Guidance literature:: Multi-step reaction with 4 steps

1: 64 percent / IBX / dimethylsulfoxide / 3 h / 20 °C

2: 96 percent / tetrahydrofuran; cyclohexane; diethyl ether / 2 h / -50 °C

3: 60 percent / triethylamine; 4-(N,N-dimethylamino)pyridine / CH₂Cl₂ / 12 h / 20 °C

4: 68 percent / LiBr; CuI / tetrahydrofuran; diethyl ether / 0.67 h / 0 °C

With dmap; copper(l) iodide; triethylamine; lithium bromide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; diethyl ether; dichloromethane; cyclohexane; dimethyl sulfoxide;
DOI:10.1002/ejoc.200500096

Reference yield:

: 861721-83-7
1,3-bis(4-bromophenyl)-1-phenylprop-2-yn-1-ol

: 861721-84-8
1-bromo-4-[3-(4-bromophenyl)-1-(1,1-dimethylethyl)-3-phenylpropa-1,2-dienyl]benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / triethylamine; 4-(N,N-dimethylamino)pyridine / CH₂Cl₂ / 12 h / 20 °C

2: 68 percent / LiBr; CuI / tetrahydrofuran; diethyl ether / 0.67 h / 0 °C

With dmap; copper(l) iodide; triethylamine; lithium bromide; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1002/ejoc.200500096