(R)-1-(3-(tert-butyldimethylsilyloxy)benzyl)-5-oxo-3-(tetrahydro-2H-pyran-2-yloxy)-cyclopentene

Base Information

Chemical Name:(R)-1-(3-(tert-butyldimethylsilyloxy)benzyl)-5-oxo-3-(tetrahydro-2H-pyran-2-yloxy)-cyclopentene
CAS No.:1425937-60-5
Molecular Formula:C₂₃H₃₄O₄Si
Molecular Weight:402.606
Hs Code.:

Synonyms:(R)-1-(3-(tert-butyldimethylsilyloxy)benzyl)-5-oxo-3-(tetrahydro-2H-pyran-2-yloxy)-cyclopentene

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Chemical Property of (R)-1-(3-(tert-butyldimethylsilyloxy)benzyl)-5-oxo-3-(tetrahydro-2H-pyran-2-yloxy)-cyclopentene

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Technology Process of (R)-1-(3-(tert-butyldimethylsilyloxy)benzyl)-5-oxo-3-(tetrahydro-2H-pyran-2-yloxy)-cyclopentene

There total 9 articles about (R)-1-(3-(tert-butyldimethylsilyloxy)benzyl)-5-oxo-3-(tetrahydro-2H-pyran-2-yloxy)-cyclopentene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₇H₂₀O₄

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1425937-60-5
(R)-1-(3-(tert-butyldimethylsilyloxy)benzyl)-5-oxo-3-(tetrahydro-2H-pyran-2-yloxy)-cyclopentene

Guidance literature:: With 1H-imidazole; In ethyl acetate; at 50 ℃; for 4h;

Reference yield:

: C₂₄H₂₆O₄

: 1425937-60-5
(R)-1-(3-(tert-butyldimethylsilyloxy)benzyl)-5-oxo-3-(tetrahydro-2H-pyran-2-yloxy)-cyclopentene

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen; palladium on activated charcoal / ethanol / 2 h / 20 °C

2: 1H-imidazole / ethyl acetate / 4 h / 50 °C

With 1H-imidazole; palladium on activated charcoal; hydrogen; In ethanol; ethyl acetate;

Reference yield:

: 1417694-57-5
(R)-4-hydroxy-2-(3-benzyloxybenzyl)cyclopent-2-enone

: 1425937-60-5
(R)-1-(3-(tert-butyldimethylsilyloxy)benzyl)-5-oxo-3-(tetrahydro-2H-pyran-2-yloxy)-cyclopentene

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / dichloromethane / 10 - 20 °C

2: hydrogen; palladium on activated charcoal / ethanol / 2 h / 20 °C

3: 1H-imidazole / ethyl acetate / 4 h / 50 °C

With 1H-imidazole; palladium on activated charcoal; hydrogen; toluene-4-sulfonic acid; In ethanol; dichloromethane; ethyl acetate;