(1S,8R,9R,10R)-8-phenyl-1-decalyl (S)-[(1-phenylethyl)carbamoyl] phthalate

Base Information

Chemical Name:(1S,8R,9R,10R)-8-phenyl-1-decalyl (S)-[(1-phenylethyl)carbamoyl] phthalate
CAS No.:191278-15-6
Molecular Formula:C₃₂H₃₅NO₃
Molecular Weight:481.635
Hs Code.:

Synonyms:(1S,8R,9R,10R)-8-phenyl-1-decalyl (S)-[(1-phenylethyl)carbamoyl] phthalate

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Chemical Property of (1S,8R,9R,10R)-8-phenyl-1-decalyl (S)-[(1-phenylethyl)carbamoyl] phthalate

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Technology Process of (1S,8R,9R,10R)-8-phenyl-1-decalyl (S)-[(1-phenylethyl)carbamoyl] phthalate

There total 3 articles about (1S,8R,9R,10R)-8-phenyl-1-decalyl (S)-[(1-phenylethyl)carbamoyl] phthalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 2627-86-3
(S)-1-phenyl-ethylamine

: (1S*,8R*,9R*,10R*)-8-phenyl-1-decalyl hydrogen phthalate

: (1R,8S,9S,10S)-8-phenyl-1-decalyl (S)-[(1-phenylethyl)carbamoyl] phthalate

: 191278-15-6
(1S,8R,9R,10R)-8-phenyl-1-decalyl (S)-[(1-phenylethyl)carbamoyl] phthalate

Guidance literature:: With diethyl cyanophosphonate; triethylamine; In N,N-dimethyl-formamide; 1.) 0 deg C, 30 min, 2.) room temperature, 5 h;
DOI:10.1021/jo970082i

Reference yield:

: 85-44-9
phthalic anhydride

: 191278-15-6
(1S,8R,9R,10R)-8-phenyl-1-decalyl (S)-[(1-phenylethyl)carbamoyl] phthalate

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / pyridine / 4 h / Heating

2: 35 percent / diethyl cyanophosphate, Et₃N / dimethylformamide / 1.) 0 deg C, 30 min, 2.) room temperature, 5 h

With diethyl cyanophosphonate; triethylamine; In pyridine; N,N-dimethyl-formamide;
DOI:10.1021/jo970082i

Reference yield:

: 104197-81-1
(1S*,8R*,9R*,10R*)-8-phenyl-1-decalol

: 191278-15-6
(1S,8R,9R,10R)-8-phenyl-1-decalyl (S)-[(1-phenylethyl)carbamoyl] phthalate

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / pyridine / 4 h / Heating

2: 35 percent / diethyl cyanophosphate, Et₃N / dimethylformamide / 1.) 0 deg C, 30 min, 2.) room temperature, 5 h

With diethyl cyanophosphonate; triethylamine; In pyridine; N,N-dimethyl-formamide;
DOI:10.1021/jo970082i