((1R,2R,3R,4S,5S)-4-amino-2,3,5-trihydroxycyclohexyl)methyl dihydrogen phosphate

Base Information

Chemical Name:((1R,2R,3R,4S,5S)-4-amino-2,3,5-trihydroxycyclohexyl)methyl dihydrogen phosphate
CAS No.:1301234-92-3
Molecular Formula:C₇H₁₆NO₇P
Molecular Weight:257.18
Hs Code.:

Synonyms:((1R,2R,3R,4S,5S)-4-amino-2,3,5-trihydroxycyclohexyl)methyl dihydrogen phosphate

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Chemical Property of ((1R,2R,3R,4S,5S)-4-amino-2,3,5-trihydroxycyclohexyl)methyl dihydrogen phosphate

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Technology Process of ((1R,2R,3R,4S,5S)-4-amino-2,3,5-trihydroxycyclohexyl)methyl dihydrogen phosphate

There total 4 articles about ((1R,2R,3R,4S,5S)-4-amino-2,3,5-trihydroxycyclohexyl)methyl dihydrogen phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1301234-99-0
(1S,2S,3R,4R,5R)-3,4-di-O-benzyl-2-benzylamino-5-((phosphonooxy)methyl)cyclohexane-1,3,4-triole

: 1301234-92-3
((1R,2R,3R,4S,5S)-4-amino-2,3,5-trihydroxycyclohexyl)methyl dihydrogen phosphate

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In methanol; at 20 ℃; for 4h;

Reference yield: 97.0%

: sodium benzyl ((1R,2R,3R,4S,5S)-4-(benzylamino)-2,3-bis(benzyloxy)-5-hydroxycyclohexyl)methyl phosphate

: 1301234-92-3
((1R,2R,3R,4S,5S)-4-amino-2,3,5-trihydroxycyclohexyl)methyl dihydrogen phosphate

Guidance literature:: With 10% Pd/C; hydrogen; In methanol; at 20 ℃; for 48h; under 3040.2 Torr;
DOI:10.1016/j.tet.2012.09.015

Reference yield:

: 106265-22-9
(1S,2S,3R,4R,5R)-3,4-di-O-benzyl-2-benzylamino-1,2-N,O-carbonyl-5-C-hydroxymethyl-1,3,4-cyclohexanetriol

: 1301234-92-3
((1R,2R,3R,4S,5S)-4-amino-2,3,5-trihydroxycyclohexyl)methyl dihydrogen phosphate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / ethanol / 14 h / Reflux

2: pyridine; water; trichlorophosphate / acetonitrile / 8.5 h / 0 °C

3: hydrogen / palladium 10% on activated carbon / methanol / 4 h / 20 °C

With pyridine; water; hydrogen; sodium hydroxide; trichlorophosphate; palladium 10% on activated carbon; In methanol; ethanol; acetonitrile;