(1S,2S,3R,4R,5R)-3,4-di-O-benzyl-2-benzylamino-5-((phosphonooxy)methyl)cyclohexane-1,3,4-triole

Base Information

Chemical Name:(1S,2S,3R,4R,5R)-3,4-di-O-benzyl-2-benzylamino-5-((phosphonooxy)methyl)cyclohexane-1,3,4-triole
CAS No.:1301234-99-0
Molecular Formula:C₂₈H₃₄NO₇P
Molecular Weight:527.554
Hs Code.:

Synonyms:(1S,2S,3R,4R,5R)-3,4-di-O-benzyl-2-benzylamino-5-((phosphonooxy)methyl)cyclohexane-1,3,4-triole

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Chemical Property of (1S,2S,3R,4R,5R)-3,4-di-O-benzyl-2-benzylamino-5-((phosphonooxy)methyl)cyclohexane-1,3,4-triole

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Technology Process of (1S,2S,3R,4R,5R)-3,4-di-O-benzyl-2-benzylamino-5-((phosphonooxy)methyl)cyclohexane-1,3,4-triole

There total 3 articles about (1S,2S,3R,4R,5R)-3,4-di-O-benzyl-2-benzylamino-5-((phosphonooxy)methyl)cyclohexane-1,3,4-triole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

: 143465-64-9
(1S,2S,3R,4R,5R)-3,4-di-O-benzyl-2-benzylamino-5-C-hydroxymethyl-1,3,4-cyclohexanetriol

: 1301234-99-0
(1S,2S,3R,4R,5R)-3,4-di-O-benzyl-2-benzylamino-5-((phosphonooxy)methyl)cyclohexane-1,3,4-triole

Guidance literature:: With pyridine; water; trichlorophosphate; In acetonitrile; at 0 ℃; for 8.5h;

Reference yield:

: 106265-22-9
(1S,2S,3R,4R,5R)-3,4-di-O-benzyl-2-benzylamino-1,2-N,O-carbonyl-5-C-hydroxymethyl-1,3,4-cyclohexanetriol

: 1301234-99-0
(1S,2S,3R,4R,5R)-3,4-di-O-benzyl-2-benzylamino-5-((phosphonooxy)methyl)cyclohexane-1,3,4-triole

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / ethanol / 14 h / Reflux

2: pyridine; water; trichlorophosphate / acetonitrile / 8.5 h / 0 °C

With pyridine; water; sodium hydroxide; trichlorophosphate; In ethanol; acetonitrile;

Reference yield:

: 106295-31-2
1D-(1,2,4,5/3)-3,4-di-O-benzyl-2-benzylamino-1,2-N,O-carbonyl-5-C-hydroxy-methyl-1,3,4-cyclohexanetriol

: 1301234-99-0
(1S,2S,3R,4R,5R)-3,4-di-O-benzyl-2-benzylamino-5-((phosphonooxy)methyl)cyclohexane-1,3,4-triole

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / ethanol / 14 h / Reflux

2: pyridine; water; trichlorophosphate / acetonitrile / 9.5 h / 0 - 20 °C

With pyridine; water; sodium hydroxide; trichlorophosphate; In ethanol; acetonitrile;