4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyloxycarbonyl chloride

Base Information

• Chemical Name: 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyloxycarbonyl chloride
• CAS No.: 1334019-92-9
• Molecular Formula: C₁₄H₁₈BClO₄
• Molecular Weight: 296.559

Synonyms:4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyloxycarbonyl chloride

Chemical Property of 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyloxycarbonyl chloride

Chemical Property:

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Technology Process of 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyloxycarbonyl chloride

There total 2 articles about 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyloxycarbonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

phosgene (75-44-5) + (4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)methanol (302348-51-2) → 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyloxycarbonyl chloride (1334019-92-9)

Guidance literature:

In tetrahydrofuran; toluene; at 20 ℃; for 24h; Inert atmosphere;

Reference yield:

1,1,1,3,3,3-hexachloro-propan-2-one (116-16-5) + (4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)methanol (302348-51-2) → 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyloxycarbonyl chloride (1334019-92-9)

Guidance literature:

With pyridine; In tetrahydrofuran; at 0 ℃;

Reference yield: 78.0%

4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyloxycarbonyl chloride (1334019-92-9) + 3-benzothiazol-2-yl-7-hydroxy-chromen-2-one (58851-99-3) → C30H26BNO7S

Guidance literature:

With triethylamine; In dichloromethane; at 0 ℃;

DOI:10.1016/j.jphotochem.2021.113270

upstream raw materials:

phosgene

(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)methanol

1,1,1,3,3,3-hexachloro-propan-2-one

Downstream raw materials:

4-hydroxybenzyl carbamate

Peroxy Naphthalene 1

4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl (2,2-dimethyl-1-(3-((4-methyl-2-oxo-2H-chromen-7-yl)oxy)propoxy)propyl)carbamate

4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl N-[(2,2-dimethyl-1-(neopentyloxy)propyl)]carbamate

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