13-Methoxy-10-methyl-12-oxo-2,5-diphenyl-12H-7,9-dioxa-3,4,6-triazabenzonaphthacene

Base Information

• Chemical Name: 13-Methoxy-10-methyl-12-oxo-2,5-diphenyl-12H-7,9-dioxa-3,4,6-triazabenzonaphthacene
• CAS No.: 84735-08-0
• Molecular Formula: C₃₀H₁₉N₃O₄
• Molecular Weight: 485.499
• Mol file: 84735-08-0.mol

Synonyms:13-Methoxy-10-methyl-12-oxo-2,5-diphenyl-12H-7,9-dioxa-3,4,6-triazabenzonaphthacene

Chemical Property of 13-Methoxy-10-methyl-12-oxo-2,5-diphenyl-12H-7,9-dioxa-3,4,6-triazabenzonaphthacene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 13-Methoxy-10-methyl-12-oxo-2,5-diphenyl-12H-7,9-dioxa-3,4,6-triazabenzonaphthacene

There total 6 articles about 13-Methoxy-10-methyl-12-oxo-2,5-diphenyl-12H-7,9-dioxa-3,4,6-triazabenzonaphthacene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

4-Amino-5-imino-12-methoxy-9-methyl-11-oxo-2-phenyl-5H,11H-pyrano<3',2':6,7><1>benzopyrano<3,4-c>pyridine (84735-01-3) + benzaldehyde (100-52-7) → 13-Methoxy-10-methyl-12-oxo-2,5-diphenyl-12H-7,9-dioxa-3,4,6-triazabenzonaphthacene (84735-08-0)

Guidance literature:

With ammonium acetate; In ethanol; for 0.5h; Heating;

DOI:10.1055/s-1982-30074

Reference yield:

2-methyl-2-phenyl[1,3]dithiolane (5769-02-8) → 13-Methoxy-10-methyl-12-oxo-2,5-diphenyl-12H-7,9-dioxa-3,4,6-triazabenzonaphthacene (84735-08-0)

Guidance literature:

Multi-step reaction with 3 steps

2: 65 percent / ammonium acetate / ethanol / 1 h / Heating

3: 70 percent / ammonium acetate / ethanol / 0.5 h / Heating

With ammonium acetate; In ethanol;

DOI:10.1055/s-1982-30074

Reference yield:

7-hydroxy-5-methoxy-2-methyl-4-oxo-4H-chromene-6-carbaldehyde (7338-51-4) → 13-Methoxy-10-methyl-12-oxo-2,5-diphenyl-12H-7,9-dioxa-3,4,6-triazabenzonaphthacene (84735-08-0)

Guidance literature:

Multi-step reaction with 3 steps

1: 85 percent / ammonium acetate / ethanol / 1 h

2: 65 percent / ammonium acetate / ethanol / 1 h / Heating

3: 70 percent / ammonium acetate / ethanol / 0.5 h / Heating

With ammonium acetate; In ethanol;

DOI:10.1055/s-1982-30074

upstream raw materials:

4-Amino-5-imino-12-methoxy-9-methyl-11-oxo-2-phenyl-5H,11H-pyrano<3',2':6,7><1>benzopyrano<3,4-c>pyridine

benzaldehyde

2-methyl-2-phenyl[1,3]dithiolane

7-hydroxy-5-methoxy-2-methyl-4-oxo-4H-chromene-6-carbaldehyde