3-(2-phenyl-1,2,3,4-tetrahydro-isoquinolin-1-yl)-1H-indole-6-carboxylic-acid methyl ester

Base Information

Chemical Name:3-(2-phenyl-1,2,3,4-tetrahydro-isoquinolin-1-yl)-1H-indole-6-carboxylic-acid methyl ester
CAS No.:1439904-93-4
Molecular Formula:C₂₅H₂₂N₂O₂
Molecular Weight:382.462
Hs Code.:

Synonyms:3-(2-phenyl-1,2,3,4-tetrahydro-isoquinolin-1-yl)-1H-indole-6-carboxylic-acid methyl ester

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Chemical Property of 3-(2-phenyl-1,2,3,4-tetrahydro-isoquinolin-1-yl)-1H-indole-6-carboxylic-acid methyl ester

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Technology Process of 3-(2-phenyl-1,2,3,4-tetrahydro-isoquinolin-1-yl)-1H-indole-6-carboxylic-acid methyl ester

There total 4 articles about 3-(2-phenyl-1,2,3,4-tetrahydro-isoquinolin-1-yl)-1H-indole-6-carboxylic-acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 50820-65-0
indole-6-carboxylic acid methyl ester

: 3340-78-1
2-phenyl-1,2,3,4-tetrahydroisoquinoline

: 1439904-93-4
3-(2-phenyl-1,2,3,4-tetrahydro-isoquinolin-1-yl)-1H-indole-6-carboxylic-acid methyl ester

Guidance literature:: With AIE-active tetraphenylethene-functionalized UiO-isoreticular zirconium metal-organic framework; In methanol; at 20 ℃; for 12h; Irradiation;
DOI:10.1039/c6cc04997d

Reference yield: 67.0%

: 1439904-93-4
3-(2-phenyl-1,2,3,4-tetrahydro-isoquinolin-1-yl)-1H-indole-6-carboxylic-acid methyl ester

Guidance literature:: With [Co(dimethylglyoxime)2Cl₂]; Eosin Y; In water; acetonitrile; at 40 ℃; for 16h; Irradiation; Inert atmosphere;

Reference yield:

: 91-21-4
1,2,3,4-tetrahydroisoquinoline

: 1439904-93-4
3-(2-phenyl-1,2,3,4-tetrahydro-isoquinolin-1-yl)-1H-indole-6-carboxylic-acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide; potassium phosphate / isopropyl alcohol / 24 h / 90 °C / Schlenk technique; Inert atmosphere

2: C₃₈H₂₆N₃OPt⁽¹⁺⁾*ClO₄^(1-)*0.5H₂O; iron(II) sulfate / N,N-dimethyl-formamide / 6 h / 20 °C / Irradiation

With potassium phosphate; copper(l) iodide; C₃₈H₂₆N₃OPt⁽¹⁺⁾*ClO₄^(1-)*0.5H₂O; iron(II) sulfate; In N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1002/chem.201204572