[MnCl((C₅H₂N(C₆H₂(CH₃)3))3(C₅H₂N(C₆H₂(C(CH₃)3)(O)(C(CH₃)2)C₆H₂(C(CH₃)3)CO₂H)))]

Base Information

Chemical Name:[MnCl((C₅H₂N(C₆H₂(CH₃)3))3(C₅H₂N(C₆H₂(C(CH₃)3)(O)(C(CH₃)2)C₆H₂(C(CH₃)3)CO₂H)))]
CAS No.:499219-43-1
Molecular Formula:C₇₁H₇₀ClMnN₄O₃
Molecular Weight:1117.75
Hs Code.:

[MnCl((C<sub>5</sub>H<sub>2</sub>N(C<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)3))3(C<sub>5</sub>H<sub>2</sub>N(C<sub>6</sub>H<sub>2</sub>(C(CH<sub>3</sub>)3)(O)(C(CH<sub>3</sub>)2)C<sub>6</sub>H<sub>2</sub>(C(CH<sub>3</sub>)3)CO<sub>2</sub>H)))]

Synonyms:[MnCl((C₅H₂N(C₆H₂(CH₃)3))3(C₅H₂N(C₆H₂(C(CH₃)3)(O)(C(CH₃)2)C₆H₂(C(CH₃)3)CO₂H)))]

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Chemical Property of [MnCl((C₅H₂N(C₆H₂(CH₃)3))3(C₅H₂N(C₆H₂(C(CH₃)3)(O)(C(CH₃)2)C₆H₂(C(CH₃)3)CO₂H)))]

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Technology Process of [MnCl((C₅H₂N(C₆H₂(CH₃)3))3(C₅H₂N(C₆H₂(C(CH₃)3)(O)(C(CH₃)2)C₆H₂(C(CH₃)3)CO₂H)))]

There total 1 articles about [MnCl((C₅H₂N(C₆H₂(CH₃)3))3(C₅H₂N(C₆H₂(C(CH₃)3)(O)(C(CH₃)2)C₆H₂(C(CH₃)3)CO₂H)))] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 7647-01-0,15364-23-5
hydrogenchloride

: 5-[4-(5-hydroxycarbonyl-2,7-di-tert-butyl-9,9-dimethylxanthenyl)]-10,15,20-trimesitylporphyrin

: 6156-78-1
manganese (II) acetate tetrahydrate

: 499219-43-1
[MnCl((C₅H₂N(C₆H₂(CH₃)3))3(C₅H₂N(C₆H₂(C(CH₃)3)(O)(C(CH₃)2)C₆H₂(C(CH₃)3)CO₂H)))]

Guidance literature:: With air; sodium chloride; In N,N-dimethyl-formamide; soln. of porphyrin and Mn compd. in DMF was refluxed in air for 3 h; cooled to room temp.; evapd.; residue taken up in CH2Cl2/water (1/1); org. layer septd.; washed (water); stirred with satd. aq. NaCl/HCl (5/1) for 90 min; org. layer decanted; solvent removed (vac.); residue chromd. (silica gel, CH2Cl2, MeOH/CH2Cl2); retreated with aq. NaCl/HCl; org. phase septd.; washed (water); dried (Na2SO4); evapd.; recrystd. (CH2Cl2/hexane); elem.anal.;
DOI:10.1021/ja028548o