C₁₅H₁₈BrNO

Base Information

Chemical Name:C₁₅H₁₈BrNO
CAS No.:1366440-28-9
Molecular Formula:C₁₅H₁₈BrNO
Molecular Weight:308.218
Hs Code.:

Synonyms:C₁₅H₁₈BrNO

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Chemical Property of C₁₅H₁₈BrNO

Chemical Property:

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Technology Process of C₁₅H₁₈BrNO

There total 5 articles about C₁₅H₁₈BrNO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 77255-26-6,2137065-16-6
trans-2-(4-bromophenyl)cyclopropanecarboxylic acid

: 765-38-8,41720-98-3,59335-84-1,79171-53-2
(S)-2-methylpyrrolidine

: 1366440-28-9
C₁₅H₁₈BrNO

Guidance literature:: trans-2-(4-bromophenyl)cyclopropanecarboxylic acid; With 1,1'-carbonyldiimidazole; In tetrahydrofuran; at 20 ℃; for 0.5h;

(S)-2-methylpyrrolidine; In tetrahydrofuran; at 15 - 20 ℃;

Reference yield:

: 1122-91-4
4-bromo-benzaldehyde

: 1366440-28-9
C₁₅H₁₈BrNO

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / toluene / 0.33 h / 5 °C

1.2: 10 - 20 °C

2.1: sodium t-butanolate / dimethyl sulfoxide; N,N-dimethyl acetamide / 0.5 h / 20 °C

2.2: 50 °C

3.1: water; lithium hydroxide / tetrahydrofuran; methanol / 3 h / 50 - 65 °C

3.2: 0.5 h / 20 °C / pH < 2

4.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 0.5 h / 20 °C

4.2: 15 - 20 °C

With water; sodium hydride; 1,1'-carbonyldiimidazole; lithium hydroxide; sodium t-butanolate; In tetrahydrofuran; methanol; N,N-dimethyl acetamide; dimethyl sulfoxide; toluene;

Reference yield:

: 1366440-18-7
tert-butyl 2-(4-bromophenyl)cyclopropanecarboxylate

: 1366440-28-9
C₁₅H₁₈BrNO

Guidance literature:: Multi-step reaction with 2 steps

1.1: water; lithium hydroxide / tetrahydrofuran; methanol / 3 h / 50 - 65 °C

1.2: 0.5 h / 20 °C / pH < 2

2.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 0.5 h / 20 °C

2.2: 15 - 20 °C

With water; 1,1'-carbonyldiimidazole; lithium hydroxide; In tetrahydrofuran; methanol;