(2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)pent-2-ene)ZnMe

Base Information

• Chemical Name: (2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)pent-2-ene)ZnMe
• CAS No.: 359641-97-7
• Molecular Formula: C₃₀H₄₄N₂Zn
• Molecular Weight: 498.083

Synonyms:(2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)pent-2-ene)ZnMe

Chemical Property of (2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)pent-2-ene)ZnMe

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Technology Process of (2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)pent-2-ene)ZnMe

There total 3 articles about (2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)pent-2-ene)ZnMe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

(2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)pent-2-ene)ZnCl (359641-96-6) + methyllithium (917-54-4) → (2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)pent-2-ene)ZnMe (359641-97-7)

Guidance literature:

In diethyl ether; under N2 atm. soln. MeLi in Et2O was slowly added to soln. (dipp)NacNacZnCl in Et2O at -78°C, mixt. was allowed to warm to room temp. andstirred for 3 h; react. mixt. was filtered, concd., and stored overnight at -24°C;elem. anal.;

DOI:10.1021/om010301x

Reference yield: 83.0%

N,N′-bis(2,6-diisopropylphenyl)pentane-2,4-diimine (210832-39-6) + dimethyl zinc(II) (544-97-8) → (2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)pent-2-ene)ZnMe (359641-97-7)

Guidance literature:

In toluene; under N2 atm. soln. ZnMe2 in toluene was added to soln. (dipp)NacNacH intoluene at 0°C, mixt. was allowed to warm to room temp. and eflu xed for 3 days; soln. was concd. and stored overnight at -24°C; elem. anal.;

DOI:10.1021/om010301x

Reference yield:

(2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)pent-2-ene)Li*OEt2 → (2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)pent-2-ene)ZnMe (359641-97-7)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether

2: diethyl ether

In diethyl ether;

DOI:10.1021/om010301x

upstream raw materials:

N,N′-bis(2,6-diisopropylphenyl)pentane-2,4-diimine

dimethyl zinc(II)

(2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)pent-2-ene)ZnCl

methyllithium

Downstream raw materials:

[N,N'-bis(2,6-diisopropylphenyl)-β-diketiminato](trifluoromethanesulfonato)zinc(II) - tetrahydrofurane (1/1)

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