(1S)-1-carboxy-2-(4-(carboxy(4,5-dimethoxy-2-nitrophenyl)methoxy)phenyl)ethanaminium 2,2,2-trifluoroacetate

Base Information

Chemical Name:(1S)-1-carboxy-2-(4-(carboxy(4,5-dimethoxy-2-nitrophenyl)methoxy)phenyl)ethanaminium 2,2,2-trifluoroacetate
CAS No.:1373931-78-2
Molecular Formula:C₂HF₃O₂*C₁₉H₂₀N₂O₉
Molecular Weight:534.4
Hs Code.:

Synonyms:(1S)-1-carboxy-2-(4-(carboxy(4,5-dimethoxy-2-nitrophenyl)methoxy)phenyl)ethanaminium 2,2,2-trifluoroacetate

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Chemical Property of (1S)-1-carboxy-2-(4-(carboxy(4,5-dimethoxy-2-nitrophenyl)methoxy)phenyl)ethanaminium 2,2,2-trifluoroacetate

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Technology Process of (1S)-1-carboxy-2-(4-(carboxy(4,5-dimethoxy-2-nitrophenyl)methoxy)phenyl)ethanaminium 2,2,2-trifluoroacetate

There total 3 articles about (1S)-1-carboxy-2-(4-(carboxy(4,5-dimethoxy-2-nitrophenyl)methoxy)phenyl)ethanaminium 2,2,2-trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1233875-87-0
α-bromo-4,5-dimethoxy-2-nitrophenylacetic acid allyl ester

: 1373931-78-2
(1S)-1-carboxy-2-(4-(carboxy(4,5-dimethoxy-2-nitrophenyl)methoxy)phenyl)ethanaminium 2,2,2-trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: caesium carbonate / tetrahydrofuran / 0.5 h / 0 °C

1.2: 20 °C

2.1: water; sodium hydroxide / tetrahydrofuran

3.1: 24 h

With water; caesium carbonate; sodium hydroxide; In tetrahydrofuran;
DOI:10.1039/c2pp05320a

Reference yield:

: 1373931-75-9
(2S)-methyl 3-(4-(2-(allyloxy)-1-(4,5-dimethoxy-2-nitrophenyl)-2-oxoethoxy)phenyl)-2-((t-butoxycarbonyl)amino)propanoate

: 1373931-78-2
(1S)-1-carboxy-2-(4-(carboxy(4,5-dimethoxy-2-nitrophenyl)methoxy)phenyl)ethanaminium 2,2,2-trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: water; sodium hydroxide / tetrahydrofuran

2: 24 h

With water; sodium hydroxide; In tetrahydrofuran;
DOI:10.1039/c2pp05320a