(2S)-methyl 3-(4-(2-(allyloxy)-1-(4,5-dimethoxy-2-nitrophenyl)-2-oxoethoxy)phenyl)-2-((t-butoxycarbonyl)amino)propanoate

Base Information

Chemical Name:(2S)-methyl 3-(4-(2-(allyloxy)-1-(4,5-dimethoxy-2-nitrophenyl)-2-oxoethoxy)phenyl)-2-((t-butoxycarbonyl)amino)propanoate
CAS No.:1373931-75-9
Molecular Formula:C₂₈H₃₄N₂O₁₁
Molecular Weight:574.585
Hs Code.:

Synonyms:(2S)-methyl 3-(4-(2-(allyloxy)-1-(4,5-dimethoxy-2-nitrophenyl)-2-oxoethoxy)phenyl)-2-((t-butoxycarbonyl)amino)propanoate

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Chemical Property of (2S)-methyl 3-(4-(2-(allyloxy)-1-(4,5-dimethoxy-2-nitrophenyl)-2-oxoethoxy)phenyl)-2-((t-butoxycarbonyl)amino)propanoate

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Technology Process of (2S)-methyl 3-(4-(2-(allyloxy)-1-(4,5-dimethoxy-2-nitrophenyl)-2-oxoethoxy)phenyl)-2-((t-butoxycarbonyl)amino)propanoate

There total 1 articles about (2S)-methyl 3-(4-(2-(allyloxy)-1-(4,5-dimethoxy-2-nitrophenyl)-2-oxoethoxy)phenyl)-2-((t-butoxycarbonyl)amino)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1233875-87-0
α-bromo-4,5-dimethoxy-2-nitrophenylacetic acid allyl ester

: 4326-36-7
(S)-N-(tert-butoxycarbonyl)tyrosine methyl ester

: 1373931-75-9
(2S)-methyl 3-(4-(2-(allyloxy)-1-(4,5-dimethoxy-2-nitrophenyl)-2-oxoethoxy)phenyl)-2-((t-butoxycarbonyl)amino)propanoate

Guidance literature:: (S)-N-(tert-butoxycarbonyl)tyrosine methyl ester; With caesium carbonate; In tetrahydrofuran; at 0 ℃; for 0.5h;

α-bromo-4,5-dimethoxy-2-nitrophenylacetic acid allyl ester; In tetrahydrofuran; at 20 ℃;
DOI:10.1039/c2pp05320a

Reference yield:

: 1373931-75-9
(2S)-methyl 3-(4-(2-(allyloxy)-1-(4,5-dimethoxy-2-nitrophenyl)-2-oxoethoxy)phenyl)-2-((t-butoxycarbonyl)amino)propanoate

: 4326-36-7
(S)-N-(tert-butoxycarbonyl)tyrosine methyl ester

Guidance literature:: In acetone; Photolysis;
DOI:10.1039/c2pp05320a

Reference yield:

: 1373931-75-9
(2S)-methyl 3-(4-(2-(allyloxy)-1-(4,5-dimethoxy-2-nitrophenyl)-2-oxoethoxy)phenyl)-2-((t-butoxycarbonyl)amino)propanoate

: 60-18-4,18875-48-4,25619-78-7,30704-25-7
L-tyrosine

Guidance literature:: Multi-step reaction with 3 steps

1: water; sodium hydroxide / tetrahydrofuran

2: 24 h

3: water-d2 / Photolysis

With water; sodium hydroxide; In tetrahydrofuran; water-d2;
DOI:10.1039/c2pp05320a