C₃₄H₅₃N₅O₆

Base Information

Chemical Name:C₃₄H₅₃N₅O₆
CAS No.:1262241-20-2
Molecular Formula:C₃₄H₅₃N₅O₆
Molecular Weight:627.825
Hs Code.:

C<sub>34</sub>H<sub>53</sub>N<sub>5</sub>O<sub>6</sub>

Synonyms:C₃₄H₅₃N₅O₆

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Chemical Property of C₃₄H₅₃N₅O₆

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Technology Process of C₃₄H₅₃N₅O₆

There total 9 articles about C₃₄H₅₃N₅O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1262241-19-9
C₄₉H₆₃N₅O₈

: 1262241-20-2
C₃₄H₅₃N₅O₆

Guidance literature:: With piperidine; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ja109377p

Reference yield:

: C₁₇H₂₅NO₃

: 1262241-20-2
C₃₄H₅₃N₅O₆

Guidance literature:: Multi-step reaction with 4 steps

1.1: tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium / decane; dichloromethane / 18 h / 4 - 20 °C / Inert atmosphere

1.2: 27 h / 4 - 20 °C

2.1: palladium 10% on activated carbon; hydrogen / 1.33 h / 20 °C / 760.05 Torr / Inert atmosphere

3.1: benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 3.5 h / 4 - 20 °C / Inert atmosphere

4.1: piperidine / dichloromethane / 2 h / 20 °C / Inert atmosphere

With piperidine; tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium; palladium 10% on activated carbon; hydrogen; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In decane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja109377p

Reference yield:

: 869487-76-3
(S)-benzyl (2,6-dimethyl-3-oxohept-1-en-4-yl)carbamate

: 1262241-20-2
C₃₄H₅₃N₅O₆

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol / 3 h / 0 °C / Inert atmosphere

2.1: tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium / decane; dichloromethane / 18 h / 4 - 20 °C / Inert atmosphere

2.2: 27 h / 4 - 20 °C

3.1: palladium 10% on activated carbon; hydrogen / 1.33 h / 20 °C / 760.05 Torr / Inert atmosphere

4.1: benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 3.5 h / 4 - 20 °C / Inert atmosphere

5.1: piperidine / dichloromethane / 2 h / 20 °C / Inert atmosphere

With piperidine; tert.-butylhydroperoxide; sodium tetrahydroborate; bis(acetylacetonate)oxovanadium; cerium(III) chloride heptahydrate; palladium 10% on activated carbon; hydrogen; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In methanol; decane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja109377p