2,3,4,6-tetra-O-acetylgalactopyranosyl-1-α-(3'-thiopropionate-O-2,3,5,6-tetrafluorophenyl ester)

Base Information

Chemical Name:2,3,4,6-tetra-O-acetylgalactopyranosyl-1-α-(3'-thiopropionate-O-2,3,5,6-tetrafluorophenyl ester)
CAS No.:158041-85-1
Molecular Formula:C₂₃H₂₄F₄O₁₁S
Molecular Weight:584.497
Hs Code.:

Synonyms:2,3,4,6-tetra-O-acetylgalactopyranosyl-1-α-(3'-thiopropionate-O-2,3,5,6-tetrafluorophenyl ester)

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Chemical Property of 2,3,4,6-tetra-O-acetylgalactopyranosyl-1-α-(3'-thiopropionate-O-2,3,5,6-tetrafluorophenyl ester)

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Technology Process of 2,3,4,6-tetra-O-acetylgalactopyranosyl-1-α-(3'-thiopropionate-O-2,3,5,6-tetrafluorophenyl ester)

There total 3 articles about 2,3,4,6-tetra-O-acetylgalactopyranosyl-1-α-(3'-thiopropionate-O-2,3,5,6-tetrafluorophenyl ester) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 79360-05-7
3-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-1-thio)propionic acid

: 142685-25-4
2,3,5,6-tetrafluorophenyl 2,2,2-trifluoroacetate

: 158041-85-1
2,3,4,6-tetra-O-acetylgalactopyranosyl-1-α-(3'-thiopropionate-O-2,3,5,6-tetrafluorophenyl ester)

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 0 ℃;
DOI:10.1021/bc100030q

Reference yield:

: 3068-32-4
1-bromo-1-deoxy-2,3,4,6-tetra-O-acetyl-a-D-galactopyranoside

: 158041-85-1
2,3,4,6-tetra-O-acetylgalactopyranosyl-1-α-(3'-thiopropionate-O-2,3,5,6-tetrafluorophenyl ester)

Guidance literature:: Multi-step reaction with 3 steps

1: acetone / 0.58 h / Reflux

2: potassium carbonate / water; acetone / 0.75 h / 20 °C

3: triethylamine / N,N-dimethyl-formamide / 0 °C

With potassium carbonate; triethylamine; In water; N,N-dimethyl-formamide; acetone;
DOI:10.1021/bc100030q

Reference yield:

: 40591-65-9,51224-13-6,51898-28-3,57030-42-9,106818-92-2
2,3,4,6-tetra-O-acetylgalactopyranosyl-1-β-pseudothiourea hydrobromide

: 158041-85-1
2,3,4,6-tetra-O-acetylgalactopyranosyl-1-α-(3'-thiopropionate-O-2,3,5,6-tetrafluorophenyl ester)

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / water; acetone / 0.75 h / 20 °C

2: triethylamine / N,N-dimethyl-formamide / 0 °C

With potassium carbonate; triethylamine; In water; N,N-dimethyl-formamide; acetone;
DOI:10.1021/bc100030q