(S)-methyl 5-[(tert-butoxycarbonyl)amino]-2-[((S)-1-cyano-2-phenylethyl)amino]-pentanoate

Base Information

Chemical Name:(S)-methyl 5-[(tert-butoxycarbonyl)amino]-2-[((S)-1-cyano-2-phenylethyl)amino]-pentanoate
CAS No.:1408237-96-6
Molecular Formula:C₂₀H₂₉N₃O₄
Molecular Weight:375.468
Hs Code.:

Synonyms:(S)-methyl 5-[(tert-butoxycarbonyl)amino]-2-[((S)-1-cyano-2-phenylethyl)amino]-pentanoate

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Chemical Property of (S)-methyl 5-[(tert-butoxycarbonyl)amino]-2-[((S)-1-cyano-2-phenylethyl)amino]-pentanoate

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Technology Process of (S)-methyl 5-[(tert-butoxycarbonyl)amino]-2-[((S)-1-cyano-2-phenylethyl)amino]-pentanoate

There total 3 articles about (S)-methyl 5-[(tert-butoxycarbonyl)amino]-2-[((S)-1-cyano-2-phenylethyl)amino]-pentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7677-24-9
trimethylsilyl cyanide

: C₁₉H₂₈N₂O₄

: 1408237-95-5
(S)-methyl 5-[(tert-butoxycarbonyl)amino]-2-[((R)-1-cyano-2-phenylethyl)amino]-pentanoate

: 1408237-96-6
(S)-methyl 5-[(tert-butoxycarbonyl)amino]-2-[((S)-1-cyano-2-phenylethyl)amino]-pentanoate

Guidance literature:: In dichloromethane; at 0 ℃;
DOI:10.1016/j.tetasy.2012.07.009

Reference yield:

: 122-78-1
phenylacetaldehyde

: 1408237-96-6
(S)-methyl 5-[(tert-butoxycarbonyl)amino]-2-[((S)-1-cyano-2-phenylethyl)amino]-pentanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 0.25 h / 20 °C

1.2: 1 h / -20 °C

2.1: dichloromethane / 0 °C

With triethylamine; In dichloromethane; 2.1: |Strecker Aminoacid Synthesis;
DOI:10.1016/j.tetasy.2012.07.009

Reference yield:

: (2S)-2-amino-5-[(tert-butoxycarbonyl)amino]pentanoic acid methylester hydrochloride

: 1408237-96-6
(S)-methyl 5-[(tert-butoxycarbonyl)amino]-2-[((S)-1-cyano-2-phenylethyl)amino]-pentanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 0.25 h / 20 °C

1.2: 1 h / -20 °C

2.1: dichloromethane / 0 °C

With triethylamine; In dichloromethane; 2.1: |Strecker Aminoacid Synthesis;
DOI:10.1016/j.tetasy.2012.07.009