2-[2-(2-{4-[Tris-(4-tert-butyl-phenyl)-methyl]-phenoxy}-ethoxy)-ethoxy]-tetrahydro-pyran

Base Information

Chemical Name:2-[2-(2-{4-[Tris-(4-tert-butyl-phenyl)-methyl]-phenoxy}-ethoxy)-ethoxy]-tetrahydro-pyran
CAS No.:253600-67-8
Molecular Formula:C₄₆H₆₀O₄
Molecular Weight:676.98
Hs Code.:

Synonyms:2-[2-(2-{4-[Tris-(4-tert-butyl-phenyl)-methyl]-phenoxy}-ethoxy)-ethoxy]-tetrahydro-pyran

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Chemical Property of 2-[2-(2-{4-[Tris-(4-tert-butyl-phenyl)-methyl]-phenoxy}-ethoxy)-ethoxy]-tetrahydro-pyran

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Technology Process of 2-[2-(2-{4-[Tris-(4-tert-butyl-phenyl)-methyl]-phenoxy}-ethoxy)-ethoxy]-tetrahydro-pyran

There total 11 articles about 2-[2-(2-{4-[Tris-(4-tert-butyl-phenyl)-methyl]-phenoxy}-ethoxy)-ethoxy]-tetrahydro-pyran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 88454-93-7
2-(2'-iodoethoxy)ethyl-2-tetrahydropyranyl ether

: 143998-20-3
4-[tris-(4-tert-butylphenyl)methyl]phenol

: 253600-67-8
2-[2-(2-{4-[Tris-(4-tert-butyl-phenyl)-methyl]-phenoxy}-ethoxy)-ethoxy]-tetrahydro-pyran

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 17h;
DOI:10.1002/(SICI)1521-3765(19991105)5:11<3310::AID-CHEM3310>3.0.CO;2-R

Reference yield:

: 253185-03-4,253185-04-5
tert-butylbenzene

: 253600-67-8
2-[2-(2-{4-[Tris-(4-tert-butyl-phenyl)-methyl]-phenoxy}-ethoxy)-ethoxy]-tetrahydro-pyran

Guidance literature:: Multi-step reaction with 3 steps

1: 6 percent

2: 97 percent / 20 h / 100 °C

3: 8.30 g / KOH / butan-1-ol; H₂O / 36 h / Heating

With potassium hydroxide; In water; butan-1-ol;
DOI:10.1021/jo00066a030

Reference yield:

: 3972-65-4
1-bromo-4-tert-butylbenzene

: 253600-67-8
2-[2-(2-{4-[Tris-(4-tert-butyl-phenyl)-methyl]-phenoxy}-ethoxy)-ethoxy]-tetrahydro-pyran

Guidance literature:: Multi-step reaction with 4 steps

1: 1) Mg / 1) THF, 2 h, 2) THF, reflux, overnight

2: 94 percent / acetyl chloride / 48 h / Heating

3: 97 percent / 20 h / 100 °C

4: 8.30 g / KOH / butan-1-ol; H₂O / 36 h / Heating

With potassium hydroxide; magnesium; acetyl chloride; In water; butan-1-ol;
DOI:10.1021/jo00066a030