(CH₂)2C(C₆H₅)CH₂OSO₂CH₃

Base Information

Chemical Name:(CH₂)2C(C₆H₅)CH₂OSO₂CH₃
CAS No.:102261-80-3
Molecular Formula:C₁₁H₁₄O₃S
Molecular Weight:226.296
Hs Code.:

(CH<sub>2</sub>)2C(C<sub>6</sub>H<sub>5</sub>)CH<sub>2</sub>OSO<sub>2</sub>CH<sub>3</sub>

Synonyms:(CH₂)2C(C₆H₅)CH₂OSO₂CH₃

Suppliers and Price of (CH₂)2C(C₆H₅)CH₂OSO₂CH₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (CH₂)2C(C₆H₅)CH₂OSO₂CH₃

Chemical Property:

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Technology Process of (CH₂)2C(C₆H₅)CH₂OSO₂CH₃

There total 5 articles about (CH₂)2C(C₆H₅)CH₂OSO₂CH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 31729-66-5
1-phenyl-1-cyclopropanemethanol

: 124-63-0
methanesulfonyl chloride

: 102261-80-3
(CH₂)2C(C₆H₅)CH₂OSO₂CH₃

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 2.66667h;

Reference yield:

: 140-29-4
phenylacetonitrile

: 102261-80-3
(CH₂)2C(C₆H₅)CH₂OSO₂CH₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.25 h / 0 °C

1.2: 18 h

2.1: lithium hydroxide / water / 18 h / Reflux

3.1: sulfuric acid / 18 h / Reflux

4.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 °C

5.1: triethylamine / dichloromethane / 2 h / 0 °C

With lithium aluminium tetrahydride; sulfuric acid; sodium hydride; triethylamine; lithium hydroxide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;
DOI:10.1002/adsc.201800886

Reference yield:

: 935-44-4
1-cyano-1-phenylcyclopropane

: 102261-80-3
(CH₂)2C(C₆H₅)CH₂OSO₂CH₃

Guidance literature:: Multi-step reaction with 4 steps

1: lithium hydroxide / water / 18 h / Reflux

2: sulfuric acid / 18 h / Reflux

3: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 °C

4: triethylamine / dichloromethane / 2 h / 0 °C

With lithium aluminium tetrahydride; sulfuric acid; triethylamine; lithium hydroxide; In tetrahydrofuran; dichloromethane; water;
DOI:10.1002/adsc.201800886