(-)-(1S)-1-[(6,6-dimethyl-1-cyclohexen-1-yl)methyl]-4-hydroxy-4-methyl-2-pentynyl pivalate

Base Information

Chemical Name:(-)-(1S)-1-[(6,6-dimethyl-1-cyclohexen-1-yl)methyl]-4-hydroxy-4-methyl-2-pentynyl pivalate
CAS No.:1197241-07-8
Molecular Formula:C₂₀H₃₂O₃
Molecular Weight:320.472
Hs Code.:

Synonyms:(-)-(1S)-1-[(6,6-dimethyl-1-cyclohexen-1-yl)methyl]-4-hydroxy-4-methyl-2-pentynyl pivalate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (-)-(1S)-1-[(6,6-dimethyl-1-cyclohexen-1-yl)methyl]-4-hydroxy-4-methyl-2-pentynyl pivalate

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Technology Process of (-)-(1S)-1-[(6,6-dimethyl-1-cyclohexen-1-yl)methyl]-4-hydroxy-4-methyl-2-pentynyl pivalate

There total 1 articles about (-)-(1S)-1-[(6,6-dimethyl-1-cyclohexen-1-yl)methyl]-4-hydroxy-4-methyl-2-pentynyl pivalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1197241-05-6
(-)-(2S)-1-(6,6-dimethyl-1-cyclohexen-1-yl)-5-methyl-3-hexyne-2,5-diol

: 3282-30-2
pivaloyl chloride

: 1197241-07-8
(-)-(1S)-1-[(6,6-dimethyl-1-cyclohexen-1-yl)methyl]-4-hydroxy-4-methyl-2-pentynyl pivalate

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃; for 15h; optical yield given as %ee;
DOI:10.1002/chem.200901292

Reference yield: 85.0%

: 1197241-07-8
(-)-(1S)-1-[(6,6-dimethyl-1-cyclohexen-1-yl)methyl]-4-hydroxy-4-methyl-2-pentynyl pivalate

: 899421-04-6
(-)-(1S)-1-[(6,6-dimethyl-1-cyclohexen-1-yl)methyl]-2-propynyl pivalate

Guidance literature:: With 18-crown-6 ether; potassium carbonate; In toluene; for 24h; optical yield given as %ee; Reflux;
DOI:10.1002/chem.200901292