(1'S,2R)-2-(1'-Methyl-2'-oxo-2'-phenylmethoxy-ethylamino)-4-oxo-4-phenyl-buttersaeure-ethylester

Base Information

Chemical Name:(1'S,2R)-2-(1'-Methyl-2'-oxo-2'-phenylmethoxy-ethylamino)-4-oxo-4-phenyl-buttersaeure-ethylester
CAS No.:134206-11-4
Molecular Formula:C₂₂H₂₅NO₅
Molecular Weight:383.444
Hs Code.:

Synonyms:(1'S,2R)-2-(1'-Methyl-2'-oxo-2'-phenylmethoxy-ethylamino)-4-oxo-4-phenyl-buttersaeure-ethylester

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Chemical Property of (1'S,2R)-2-(1'-Methyl-2'-oxo-2'-phenylmethoxy-ethylamino)-4-oxo-4-phenyl-buttersaeure-ethylester

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Technology Process of (1'S,2R)-2-(1'-Methyl-2'-oxo-2'-phenylmethoxy-ethylamino)-4-oxo-4-phenyl-buttersaeure-ethylester

There total 2 articles about (1'S,2R)-2-(1'-Methyl-2'-oxo-2'-phenylmethoxy-ethylamino)-4-oxo-4-phenyl-buttersaeure-ethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 17831-01-5
H-Ala-OBzl

: 15121-89-8
ethyl (E)-4-oxo-4-phenyl-2-butenoate

: 134206-11-4
(1'S,2R)-2-(1'-Methyl-2'-oxo-2'-phenylmethoxy-ethylamino)-4-oxo-4-phenyl-buttersaeure-ethylester

: 87269-98-5
(1'S,2S)-2-(1'-Methyl-2'-oxo-2'-phenylmethoxy-ethylamino)-4-oxo-4-phenyl-buttersaeure-ethylester

Guidance literature:: With triethylamine; In ethanol; Ambient temperature;
DOI:10.1016/S0040-4039(01)91545-X

Reference yield:

: 15121-89-8
ethyl (E)-4-oxo-4-phenyl-2-butenoate

: 42854-62-6
L-alanine benzyl ester p-toluenesulfonate

: 134206-11-4
(1'S,2R)-2-(1'-Methyl-2'-oxo-2'-phenylmethoxy-ethylamino)-4-oxo-4-phenyl-buttersaeure-ethylester

: 87269-98-5
(1'S,2S)-2-(1'-Methyl-2'-oxo-2'-phenylmethoxy-ethylamino)-4-oxo-4-phenyl-buttersaeure-ethylester

Guidance literature:: With sodium hydroxide; triethylamine; Yield given. Multistep reaction; 1.) methylene chloride, 2.) ethanol, 2 h;

Reference yield: 74.0%

: 134206-11-4
(1'S,2R)-2-(1'-Methyl-2'-oxo-2'-phenylmethoxy-ethylamino)-4-oxo-4-phenyl-buttersaeure-ethylester

: 84324-12-9,122076-80-6
N-<1(R)-(ethoxycarbonyl)-3-phenylpropyl>-(S)-alanine

Guidance literature:: With sulfuric acid; hydrogen; palladium on activated charcoal; In acetic acid; at 25 - 30 ℃; under 760 Torr;
DOI:10.1016/S0040-4039(01)91545-X