1-methyl-4-[5,5-diphenyl-5-(1-tricyclo[3.3.1.1.(3,7)]decyl)pentyl]piperazine

Base Information

Chemical Name:1-methyl-4-[5,5-diphenyl-5-(1-tricyclo[3.3.1.1.(3,7)]decyl)pentyl]piperazine
CAS No.:1427269-28-0
Molecular Formula:C₃₂H₄₄N₂
Molecular Weight:456.715
Hs Code.:

Synonyms:1-methyl-4-[5,5-diphenyl-5-(1-tricyclo[3.3.1.1.(3,7)]decyl)pentyl]piperazine

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Chemical Property of 1-methyl-4-[5,5-diphenyl-5-(1-tricyclo[3.3.1.1.(3,7)]decyl)pentyl]piperazine

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Technology Process of 1-methyl-4-[5,5-diphenyl-5-(1-tricyclo[3.3.1.1.(3,7)]decyl)pentyl]piperazine

There total 7 articles about 1-methyl-4-[5,5-diphenyl-5-(1-tricyclo[3.3.1.1.(3,7)]decyl)pentyl]piperazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1427163-16-3
1-methyl-4-(δ,δ-diphenyl-δ-(1-tricyclo[3.3.1.1.(3,7)]decyl)pentanoyl)piperazine

: 1427269-28-0
1-methyl-4-[5,5-diphenyl-5-(1-tricyclo[3.3.1.1.(3,7)]decyl)pentyl]piperazine

Guidance literature:: 1-methyl-4-(δ,δ-diphenyl-δ-(1-tricyclo[3.3.1.1.(3,7)]decyl)pentanoyl)piperazine; With lithium aluminium tetrahydride; In tetrahydrofuran; for 3h; Reflux;

With water; sodium hydroxide; In ethanol; at 0 ℃;
DOI:10.2174/157340612801216201

Reference yield:

: 1427162-90-0
δ,δ-diphenyl-δ-(1-tricyclo[3.3.1.1.(3,7)]decyl)butanol

: 1427269-28-0
1-methyl-4-[5,5-diphenyl-5-(1-tricyclo[3.3.1.1.(3,7)]decyl)pentyl]piperazine

Guidance literature:: Multi-step reaction with 7 steps

1.1: pyridine / dichloromethane / 12 h / 0 - 20 °C

2.1: dimethyl sulfoxide / 12 h / 60 °C / Inert atmosphere

3.1: hydrogenchloride / 2 h / Reflux

3.2: 1 h / Reflux

4.1: sodium hydroxide / ethanol; water / 2 h / Reflux

4.2: 0 °C

5.1: thionyl chloride / 1 h / Reflux

6.1: tetrahydrofuran / 3 h / Cooling; Reflux

7.1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / Reflux

7.2: 0 °C

With pyridine; hydrogenchloride; lithium aluminium tetrahydride; thionyl chloride; sodium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; water; dimethyl sulfoxide;
DOI:10.2174/157340612801216201

Reference yield:

: 66951-99-3
α,α-diphenyl-1-tricyclo[3.3.1.1.(3,7)]decanemethanol

: 1427269-28-0
1-methyl-4-[5,5-diphenyl-5-(1-tricyclo[3.3.1.1.(3,7)]decyl)pentyl]piperazine

Guidance literature:: Multi-step reaction with 9 steps

1.1: thionyl chloride; acetyl chloride / 0.5 h / Reflux

2.1: copper(l) iodide / tetrahydrofuran / 4 h / Inert atmosphere; Reflux

2.2: 0 °C / Inert atmosphere

3.1: pyridine / dichloromethane / 12 h / 0 - 20 °C

4.1: dimethyl sulfoxide / 12 h / 60 °C / Inert atmosphere

5.1: hydrogenchloride / 2 h / Reflux

5.2: 1 h / Reflux

6.1: sodium hydroxide / ethanol; water / 2 h / Reflux

6.2: 0 °C

7.1: thionyl chloride / 1 h / Reflux

8.1: tetrahydrofuran / 3 h / Cooling; Reflux

9.1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / Reflux

9.2: 0 °C

With pyridine; hydrogenchloride; copper(l) iodide; lithium aluminium tetrahydride; thionyl chloride; acetyl chloride; sodium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; water; dimethyl sulfoxide;
DOI:10.2174/157340612801216201