1-methyl-4-(δ,δ-diphenyl-δ-(1-tricyclo[3.3.1.1.(3,7)]decyl)pentanoyl)piperazine

Base Information

Chemical Name:1-methyl-4-(δ,δ-diphenyl-δ-(1-tricyclo[3.3.1.1.(3,7)]decyl)pentanoyl)piperazine
CAS No.:1427163-16-3
Molecular Formula:C₃₂H₄₂N₂O
Molecular Weight:470.698
Hs Code.:

Synonyms:1-methyl-4-(δ,δ-diphenyl-δ-(1-tricyclo[3.3.1.1.(3,7)]decyl)pentanoyl)piperazine

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Chemical Property of 1-methyl-4-(δ,δ-diphenyl-δ-(1-tricyclo[3.3.1.1.(3,7)]decyl)pentanoyl)piperazine

Chemical Property:

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Technology Process of 1-methyl-4-(δ,δ-diphenyl-δ-(1-tricyclo[3.3.1.1.(3,7)]decyl)pentanoyl)piperazine

There total 8 articles about 1-methyl-4-(δ,δ-diphenyl-δ-(1-tricyclo[3.3.1.1.(3,7)]decyl)pentanoyl)piperazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1427162-90-0
δ,δ-diphenyl-δ-(1-tricyclo[3.3.1.1.(3,7)]decyl)butanol

: 1427163-16-3
1-methyl-4-(δ,δ-diphenyl-δ-(1-tricyclo[3.3.1.1.(3,7)]decyl)pentanoyl)piperazine

Guidance literature:: Multi-step reaction with 6 steps

1.1: pyridine / dichloromethane / 12 h / 0 - 20 °C

2.1: dimethyl sulfoxide / 12 h / 60 °C / Inert atmosphere

3.1: hydrogenchloride / 2 h / Reflux

3.2: 1 h / Reflux

4.1: sodium hydroxide / ethanol; water / 2 h / Reflux

4.2: 0 °C

5.1: thionyl chloride / 1 h / Reflux

6.1: tetrahydrofuran / 3 h / Cooling; Reflux

With pyridine; hydrogenchloride; thionyl chloride; sodium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; water; dimethyl sulfoxide;
DOI:10.2174/157340612801216201

Reference yield:

: C₂₇H₃₂O₂

: 1427163-16-3
1-methyl-4-(δ,δ-diphenyl-δ-(1-tricyclo[3.3.1.1.(3,7)]decyl)pentanoyl)piperazine

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 1 h / Reflux

2: tetrahydrofuran / 3 h / Cooling; Reflux

With thionyl chloride; In tetrahydrofuran;
DOI:10.2174/157340612801216201

Reference yield:

: 66951-99-3
α,α-diphenyl-1-tricyclo[3.3.1.1.(3,7)]decanemethanol

: 1427163-16-3
1-methyl-4-(δ,δ-diphenyl-δ-(1-tricyclo[3.3.1.1.(3,7)]decyl)pentanoyl)piperazine

Guidance literature:: Multi-step reaction with 8 steps

1.1: thionyl chloride; acetyl chloride / 0.5 h / Reflux

2.1: copper(l) iodide / tetrahydrofuran / 4 h / Inert atmosphere; Reflux

2.2: 0 °C / Inert atmosphere

3.1: pyridine / dichloromethane / 12 h / 0 - 20 °C

4.1: dimethyl sulfoxide / 12 h / 60 °C / Inert atmosphere

5.1: hydrogenchloride / 2 h / Reflux

5.2: 1 h / Reflux

6.1: sodium hydroxide / ethanol; water / 2 h / Reflux

6.2: 0 °C

7.1: thionyl chloride / 1 h / Reflux

8.1: tetrahydrofuran / 3 h / Cooling; Reflux

With pyridine; hydrogenchloride; copper(l) iodide; thionyl chloride; acetyl chloride; sodium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; water; dimethyl sulfoxide;
DOI:10.2174/157340612801216201