methyl 2-[2-(2-methyl-3-(2-methylphenyl)-4(3H)-quinazolin-8-yloxy)acetyl] hydrazinecarbodithioate

Base Information

Chemical Name:methyl 2-[2-(2-methyl-3-(2-methylphenyl)-4(3H)-quinazolin-8-yloxy)acetyl] hydrazinecarbodithioate
CAS No.:1353155-70-0
Molecular Formula:C₂₀H₂₀N₄O₃S₂
Molecular Weight:428.536
Hs Code.:

Synonyms:methyl 2-[2-(2-methyl-3-(2-methylphenyl)-4(3H)-quinazolin-8-yloxy)acetyl] hydrazinecarbodithioate

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Chemical Property of methyl 2-[2-(2-methyl-3-(2-methylphenyl)-4(3H)-quinazolin-8-yloxy)acetyl] hydrazinecarbodithioate

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Technology Process of methyl 2-[2-(2-methyl-3-(2-methylphenyl)-4(3H)-quinazolin-8-yloxy)acetyl] hydrazinecarbodithioate

There total 4 articles about methyl 2-[2-(2-methyl-3-(2-methylphenyl)-4(3H)-quinazolin-8-yloxy)acetyl] hydrazinecarbodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1365839-62-8
potassium 2-[2-(2-methyl-3-(2-methylphenyl)-4(3H)-quinazolin-8-yloxy)acetyl]hydrazinecarbodithioate

: 74-88-4
methyl iodide

: 1353155-70-0
methyl 2-[2-(2-methyl-3-(2-methylphenyl)-4(3H)-quinazolin-8-yloxy)acetyl] hydrazinecarbodithioate

Guidance literature:: In ethanol; at 20 ℃; for 2h;
DOI:10.1007/s00044-011-9914-8

Reference yield:

: 1319735-77-7
2-[3,4-dihydro-2-methyl-3-(2-methylphenyl)-4-oxoquinazolin-8-yloxy]acetic acid hydrazide

: 1353155-70-0
methyl 2-[2-(2-methyl-3-(2-methylphenyl)-4(3H)-quinazolin-8-yloxy)acetyl] hydrazinecarbodithioate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / ethanol / 3 h / 20 °C

2: ethanol / 2 h / 20 °C

With potassium hydroxide; In ethanol;
DOI:10.1016/j.bmcl.2011.11.007

Reference yield:

: 1319735-76-6
ethyl 2-[3,4-dihydro-2-methyl-3-(2-methylphenyl)-4-oxoquinazolin-8-yloxy]acetate

: 1353155-70-0
methyl 2-[2-(2-methyl-3-(2-methylphenyl)-4(3H)-quinazolin-8-yloxy)acetyl] hydrazinecarbodithioate

Guidance literature:: Multi-step reaction with 3 steps

1: hydrazine / ethanol / 20 °C

2: potassium hydroxide / ethanol / 3 h / 20 °C

3: ethanol / 2 h / 20 °C

With potassium hydroxide; hydrazine; In ethanol;
DOI:10.1016/j.bmcl.2011.11.007