(E)-6-N-t-butoxycarbonyl-2',3'-O-isopropylidene-5'-N-(5''-[2'''-(methoxycarbonyl)phenyl]-5''-oxopent-1''-ene-1''-sulfonyl)aminodeoxyadenosine

Base Information

• Chemical Name: (E)-6-N-t-butoxycarbonyl-2',3'-O-isopropylidene-5'-N-(5''-[2'''-(methoxycarbonyl)phenyl]-5''-oxopent-1''-ene-1''-sulfonyl)aminodeoxyadenosine
• CAS No.: 1094678-23-5
• Molecular Formula: C₃₁H₃₈N₆O₁₀S
• Molecular Weight: 686.743

Synonyms:(E)-6-N-t-butoxycarbonyl-2',3'-O-isopropylidene-5'-N-(5''-[2'''-(methoxycarbonyl)phenyl]-5''-oxopent-1''-ene-1''-sulfonyl)aminodeoxyadenosine

Chemical Property of (E)-6-N-t-butoxycarbonyl-2',3'-O-isopropylidene-5'-N-(5''-[2'''-(methoxycarbonyl)phenyl]-5''-oxopent-1''-ene-1''-sulfonyl)aminodeoxyadenosine

Chemical Property:

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Technology Process of (E)-6-N-t-butoxycarbonyl-2',3'-O-isopropylidene-5'-N-(5''-[2'''-(methoxycarbonyl)phenyl]-5''-oxopent-1''-ene-1''-sulfonyl)aminodeoxyadenosine

There total 1 articles about (E)-6-N-t-butoxycarbonyl-2',3'-O-isopropylidene-5'-N-(5''-[2'''-(methoxycarbonyl)phenyl]-5''-oxopent-1''-ene-1''-sulfonyl)aminodeoxyadenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butyl 9-(((3aR,4R,6R,6aR)-6-(aminomethyl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)-9H-purin-6-yl)carbamate (873556-45-7) + C13H13ClO5S (1152174-58-7) → (E)-6-N-t-butoxycarbonyl-2',3'-O-isopropylidene-5'-N-(5''-[2'''-(methoxycarbonyl)phenyl]-5''-oxopent-1''-ene-1''-sulfonyl)aminodeoxyadenosine (1094678-23-5)

Guidance literature:

With 2,6-dimethylpyridine; In dichloromethane; at 20 ℃; for 5h;

DOI:10.1016/j.bmcl.2008.07.130

Reference yield: 88.0%

(E)-6-N-t-butoxycarbonyl-2',3'-O-isopropylidene-5'-N-(5''-[2'''-(methoxycarbonyl)phenyl]-5''-oxopent-1''-ene-1''-sulfonyl)aminodeoxyadenosine (1094678-23-5) → (E)-5'-N-(5''-[2'''-(methoxycarbonyl)phenyl]-5''-oxopent-1''-ene-1''-sulfonyl)aminodeoxyadenosine (1094678-30-4)

Guidance literature:

With trifluoroacetic acid; In water; at 0 - 20 ℃;

DOI:10.1016/j.bmcl.2008.07.130

upstream raw materials:

tert-butyl 9-(((3aR,4R,6R,6aR)-6-(aminomethyl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)-9H-purin-6-yl)carbamate

C₁₃H₁₃ClO₅S

Downstream raw materials:

(E)-5'-N-(5''-[2'''-(methoxycarbonyl)phenyl]-5''-oxopent-1''-ene-1''-sulfonyl)aminodeoxyadenosine

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